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HomeMy WebLinkAboutAttachment 8M - Phase II ESAPhase II Environmental Site Assessment Assessor’s Parcel Numbers 644-050-13 and -14 and the Western Portion of 644-050-08 821 Main Street, Chula Vista, CA 91911 Presented to: VWP-OP Nirvana Owner, LLC 2390 East Camelback Road Ste. 305 Phoenix, Arizona 85016 8799 Balboa Avenue, Suite 290 San Diego, CA 92123 858-571-5500 01221156.00 | December 7, 2021 Phase II ESA www.scsengineers.com i December 7, 2021 Number: 01221156.00 Mr. Steven Schwarz VWP-OP Nirvana Owner, LLC 2390 East Camelback Road Ste. 305 Phoenix, AZ 85016 RE: Phase II Environmental Site Assessment Site: Assessor’s Parcel Numbers (APNs) 644-050-13 and -14 and the Western Portion of 644-050-08 821 Main Street, Chula Vista, California 91911 Dear Mr. Schwarz: SCS Engineers (SCS) is pleased to present this report (Report) of the soil and soil vapor sampling and human health risk screening (Phase II Environmental Site Assessment [Phase II ESA]) of the above-described Site that was conducted in order to evaluate the Site’s current environmental conditions. The work described in this Report was performed by SCS in general accordance with Exhibit 00 to the Assignment and Assumption of Contracts (Contract) between SCS and VWP-OP Nirvana Owner, LLC (Client), fully executed on June 22, 2021, and Scope of Services Change Number 3, fully executed on November 3, 2021. SCS enjoyed working with you on this project. Providing economical environmental solutions to meet your needs is more than our goal—it is our mission and the measure of our success. If we may assist you in any way, now or in the future, please call our office at (858) 571-5500. Sincerely, Allison O’Neal Staff Professional Luke Montague, MESM, PG 8071 Vice President SCS ENGINEERS SCS ENGINEERS Phase II ESA www.scsengineers.com i Table of Contents Section Page 1 Background ................................................................................................................................... 1 2 Objectives ..................................................................................................................................... 1 3 Phase II ESA .................................................................................................................................. 2 Preparation for Fieldwork .................................................................................................................. 2 Preparation of Health and Safety Plan .................................................................................... 2 Utility Search and Markout ...................................................................................................... 2 Field Activities..................................................................................................................................... 2 Soil Vapor Sampling and Analysis ........................................................................................... 2 Soil Sampling and Analysis ...................................................................................................... 3 Soil Screening Regulatory Criteria for CoC-Bearing Soil .................................................................. 4 Health Risk-Based Mitigation Criteria ..................................................................................... 5 Waste-Based Mitigation Criteria .............................................................................................. 5 4 Findings ......................................................................................................................................... 6 Topography, Geology, Hydrogeology, and Water Quality Survey ..................................................... 6 Topography ............................................................................................................................... 6 Geology ...................................................................................................................................... 7 Hydrogeology ............................................................................................................................ 7 Water Quality Survey ................................................................................................................ 7 Laboratory Analytical Results and Screening ................................................................................... 8 Soil Vapor Sample Analytical Results ...................................................................................... 8 VOCs…….. ..................................................................................................................... 8 VOCs in Soil Vapor ....................................................................................................... 8 Vapor Intrusion Risk Screening (VIRS) .................................................................................... 9 Approach.. .................................................................................................................... 9 VIRS Results ................................................................................................................ 9 Soil Sample Analytical Results ............................................................................................. 10 Lead and Other Metals.......................................................................................................... 10 Comparison of Metals Concentrations to Waste-Based Mitigation Criteria (i.e., for Soil Export) .......................................................................................... 11 Comparison of Metals Concentrations to Risk-Based Mitigation Criteria (i.e., for Soil that Remains on-Site) ................................................................. 12 Total Petroleum Hydrocarbons (TPH) ................................................................................... 12 Comparison of TPH Concentrations to Waste-Based Mitigation Criteria (i.e., for Soil Export) .......................................................................................... 13 Comparison of TPH Concentrations to Risk-Based Mitigation Criteria (i.e., for Soil that Remains on-Site) ....................................................................... 13 Volatile Organic Compounds (VOCs) .................................................................................... 13 Polycyclic Aromatic Hydrocarbons (PAHs) ............................................................................ 14 Comparison of PAH Concentrations to Waste-Based Mitigation Criteria (i.e., for Soil Export) .......................................................................................... 14 Comparison of PAH Concentrations to Risk-Based Mitigation Criteria (i.e., for Soil that Remains on-Site) ....................................................................... 15 Phase II ESA www.scsengineers.com ii 5 Conclusions .................................................................................................................................15 Soil Investigation ...................................................................................................... 16 6 Recommendations ......................................................................................................................17 Soil Vapor Investigation ........................................................................................... 17 Soil Investigation ...................................................................................................... 17 7 Report Usage and Future Site Conditions ...................................................................................17 7 Likelihood Statements ................................................................................................................18 8 Special Contractual Conditions Between User and Environmental Professional .......................18 Tables 1 Soil Vapor Sample Analytical Results 2 Soil Sample Analytical Results for TPH, VOCs, and PAHs 3 Soil Sample Analytical Results for Metals Figures 1 Four-Way Site Location Map 2 Site Map with Soil Vapor Analytical Results 3 Site Map with Soil Sample Analytical Results Appendix A Laboratory Analytical Reports Phase II ESA www.scsengineers.com 1 1 BACKGROUND SCS Engineers (SCS) understands that 821 Main Street consists of two full parcels of land (APNs 644-050-13 & -14)and the western portion of a third parcel of land (APN 644-050-08) totaling approximately 17.11 acres of land in Chula Vista, California (Site) (Figure 1). The Site consists of a vacant hillside that is bordered by Main Street to the south, and several industrial properties to the east and upgradient of the Site, including a general contractor yard and vehicle storage and salvage lots. The Client is proposing to purchase the Site for development into an industrial land use. SCS completed a report titled Phase I Environmental Site Assessment for the Site, dated September 23, 2021 (Phase I ESA). Although the Phase I ESA did not reveal evidence of recognized environmental conditions, after discussions with the Client and the Client’s investor, the Client is requesting subsurface assessment activities for the following environmental concerns that were identified in the Phase I ESA: •On-Site drainage channels and adjacent upgradient industrial properties – two drainage channels transect the central and western portions of the Site that convey surface water from upgradient industrial properties, and portions of these drainage channels are unlined (Figures 2 and 3). The central portion of the north adjacent property at 800 to 880 Energy Way, identified as LKQ Pick Your Part that serves as an automobile maintenance/storage yard (former wrecking yard), was interpreted to drain into the central drainage system that transects the Site. The western drainage channel adjacent to the northwest tenant, FJ Willert Contracting at 1869 Nirvana Way, was obscured due to heavy vegetation. •Totes adjacent to the Site with unidentified contents – several totes with unidentified dark colored liquid and solid contents, with grassy vegetation growing from within the totes, were observed adjacent to the northern property line toward the eastern edge of the Site (Figures 2 and 3) at the time of the Phase I ESA (note that these totes were removed from the adjacent northern property at the time that subsurface assessment activities were conducted by SCS on November 11, 2021). These totes are believed to be derived from the adjacent LKQ Pick Your Part facility at 800 to 880 Energy Way. Based on the findings presented in the Phase I ESA, SCS previously collected three representative surficial soil samples from sediments within the on-Site drainage channels on July 13, 2021, and analyzed the samples for constituents of concern (CoCs) including total petroleum hydrocarbons (TPH), volatile organic compounds (VOCs), and Title 22 metals. The results of the sampling indicated detectable levels of TPH that were below health risk-based screening levels, and were transmitted to the Client within an email submittal. Based on a request from the Client’s investor and conversations with the Client, SCS has conducted the following scope of services consisting of additional shallow soil sampling as well as soil vapor sampling to additionally assess for the potential environmental concerns that were identified in the Phase I ESA associated with the drainage channels and adjacent upgradient industrial properties and totes adjacent to the Site with unidentified contents. 2 OBJECTIVES The objectives of the scope of services were to: Phase II ESA www.scsengineers.com 2 • Assess the possible presence and concentrations of CoCs (i.e., petroleum hydrocarbons, polycyclic aromatic hydrocarbons [PAHs], VOCs, and Title 22 metals) within representative locations within the on-Site drainage channels, in connection with possible impacts from the northern adjacent industrial properties. • Assess the possible presence and concentrations of VOCs in the shallow soil vapor beneath the Site in connection with possible releases from the northern adjacent industrial properties that may have impacted the Site. • Assess the likelihood that Significant 1 human health risk exists at the Site as a result of vapor phase migration of VOCs. 3 PHASE II ESA PREPARATION FOR FIELDWORK Preparation of Health and Safety Plan A health and safety plan for work conducted at the Site and workers within the “exclusion zone” is required pursuant to the regulations found in 29 Code of Federal Regulations (CFR) Part 1910.120 and California Code of Regulations (CCR), Title 8, Section 5192. Therefore, a health and safety plan was prepared for the proposed work scope, which outlined the potential chemical and physical hazards that may have been encountered during drilling and sampling activities. The appropriate personal protective equipment and emergency response procedures for the anticipated Site-specific chemical and physical hazards were detailed in this plan. SCS and contracted personnel involved with the proposed field work were required to read and sign this document in order to encourage proper health and safety practices. Utility Search and Markout SCS notified Underground Service Alert on November 4, 2021, as required by state law, prior to drilling and sampling activities and was issued ticket number B213080820. In addition, a private utility locator, Subsurface Alert, was subcontracted to clear the proposed boring locations for possible subsurface utility conflicts. These procedures were designed to minimize the likelihood of drilling into a subsurface utility. FIELD ACTIVITIES Soil Vapor Sampling and Analysis On November 11, 2021, SCS oversaw the drilling and installation of three soil vapor probes (SV1 through SV3) to assess the possible presence and concentrations of VOCs in the soil vapor in connection with possible subsurface impacts from the adjacent upgradient industrial facilities. The following table describes the proposed soil vapor sampling locations and depth. Locations of soil vapor samples are included in Figure 2. 1 For the purposes of this assessment, significant is defined as greater than one in 1,000,000 excess lifetime cancer risk or a hazard index of greater than 1. Phase II ESA www.scsengineers.com 3 Vapor Boring ID Location Sample Depth (feet bgs) Analysis SV1 Northwest corner of the Site toward the top of the western drainage channel, to assess for possible impacts from the adjacent FJ Willert Contracting at 1869 Nirvana Way 4 1 VOC SV2 Toward the center of the northern property line at the Site toward the top of the central drainage channel, to assess for possible impacts from the adjacent LKQ Pick Your Part facility at 800 to 880 Energy Way 2 1 VOC SV3, SV3-3 Rep Northeast corner of the Site adjacent to unidentified totes, to assess for possible impacts from the totes and the adjacent LKQ Pick Your Part facility at 800 to 880 Energy Way 3 2 VOCs Note: bgs: below ground surface. The soil vapor sample borings SV1 through SV3 were advanced with an electric rotohammer to the attempted depth of 5 feet below grade, although due to practical refusal encountered with the rotohammer due to stiff and rocky soil, the borings were advanced to the maximum attainable depths ranging from approximately 2 to 4 feet below grade. Note that due to the rugged and slopped nature of the Site, it was not considered feasible to use a drill rig or limited access drill rig to advance the proposed soil vapor borings. Soil vapor sampling activities were conducted in general accordance with the Department of Toxic Substances Control (DTSC), Los Angeles Regional Water Quality Control Board (RWQCB), and San Francisco RWQCB Advisory on Active Soil Gas Investigations, dated July 2015. A temporary soil vapor well, consisting of Nylaflow™ tubing attached to a soil gas probe tip, was installed near the bottom of each boring. An appropriate sand pack a minimum of 6 inches thick was placed around the soil gas probe tip, and the borings were backfilled with at least 6 inches of dry granular bentonite above each sample port, then topped with hydrated granular bentonite to the surface. The soil vapor sampling probes were allowed to stabilize for approximately 2 hours prior to sampling, followed by removing the DTSC-default of three purge volumes, and performing a shut-in test and leak test. Soil vapor samples were collected from the soil vapor sampling probes by collecting soil vapor drawn through the probes into laboratory-provided glass syringes. Soil vapor samples were delivered to an off-Site state-certified, mobile laboratory (H&P Mobile Geochemistry) and analyzed for VOCs in general accordance with U.S. Environmental Protection Agency (EPA) Method TO-15. In accordance with the DTSC guidance, one replicate sample was analyzed (SV3-3 Rep). Chain-of-custody procedures were implemented for sample tracking. Soil Sampling and Analysis On July 13, 2021, SCS collected soil samples using a trowel (borings SB1 through SB3) to the total depth of 0.5 feet below grade at the Site. On November 11, 2021, SCS advanced five additional soil borings by using a hand-held auger (borings SB4 through SB8) to total depths of up to 2.0 feet below grade at the Site, collecting soil samples at approximate depths of 0.5 feet below grade and 1 to 2 feet below grade. Locations of the soil samples are included in Figure 3. The following table summarizes the completed soil borings with depths and laboratory analysis for soil samples. Phase II ESA www.scsengineers.com 4 Boring ID Boring Location Sample Depths/ Lab Analysis Number of Samples Analyzed SB1 Within representative portions of the western drainage channel 0.5 feet: TPH, VOCs, and Title 22 Metals 1 TPH 1 VOCs 1 Metals SB2, SB3 Within representative portions of the central drainage channel 0.5 feet: TPH, VOCs, and Title 22 Metals 2 TPH 2 VOCs 2 Metals SB4, SB5, SB6 Within representative portions of the western drainage channel 0.5 feet: TPH, PAHs, and VOCs 1-1.75 feet (SB6) or 2 feet (SB4 and SB5): Archived 3 TPH 3 PAHs 3 VOCs SB7, SB8 Within representative portions of the central drainage channel 0.5 feet: TPH, PAHs, and VOCs 1-1.75 feet (SB7) and 2 feet (SB8): Archive 2 TPH 2 PAHs 2 VOCs TOTALS Soil Samples Analyses: 8 TPH, 5 PAHs, 8 VOCs, 3 Metals Notes: PAHs: Polycyclic aromatic hydrocarbons analyzed in general accordance with EPA Method 8270C SIM. TPH: Total petroleum hydrocarbons analyzed in general accordance with EPA Method 8015B. VOCs: Volatile organic compounds analyzed in general accordance with EPA Method 8260B. Title 22 Metals analyzed in general accordance with EPA Method 6010B. Soil samples were collected with the trowel or hand-held auger and were transferred directly from the blade or barrel of the hand auger with a gloved hand into a new 4-ounce glass jar. The sampling equipment was decontaminated on-Site between soil samples to minimize the likelihood of “cross-contaminating” the samples and to minimize the potential for a “false positive” in the soil samples analyzed. The soil cuttings from the hand auger borings were used to backfill the borings. The sample containers were labeled and delivered to an off-Site laboratory for analysis. Chain-of- custody procedures were implemented for sample tracking. A copy of the laboratory analytical report is provided in Appendix A. SOIL SCREENING REGULATORY CRITERIA FOR COC-BEARING SOIL Concentrations of CoCs that are reported by the laboratory in soils at the Site are compared to applicable regulatory screening values to assess whether certain soils will require segregation and proper management during Site development. There are two categories of mitigation work that will be required and are principally based upon risk- based corrective action. These categories include: o Health Risk-Based Mitigation Criteria - risk-driven remediation required by future land uses and protection of workers, and Phase II ESA www.scsengineers.com 5 o Waste-Based Mitigation Criteria - in the event that soil is exported off Site, in which case soil may be considered regulated waste provided it contains detectable concentrations of TPH, VOCs, PAHs, or elevated concentrations of metals such as lead or arsenic. Soil screening criteria are used in this Report for comparison of the reported soil sample results to applicable health risk-based and waste-based soil for the detected CoCs. The applicable soil screening applied in the “Findings” section below includes the following: Health Risk-Based Mitigation Criteria For health risk-based screening purposes, to screen soil for possible risks to residential users and workers at the Site: • For TPH and VOCs, the San Francisco Bay Regional Water Quality Control Board (SFRWQCB) Environmental Screening Levels (ESLs) for commercial/industrial users, dated 2019, revision 2 • For SVOCs and metals, the DTSC Human and Ecological Risk Office (HERO) Human Health Risk Assessment (HHRA) Note Number 3, June 2020: Recommended Screening Levels (RSLs) for commercial/industrial soil are used. • For other PAHs where the DTSC RSLs are not established (phenanthrene), the EPA RSLs for commercial/industrial soil, November 2021, are used. Waste-Based Mitigation Criteria For waste-based screening purposes, the below criteria are applied in the event that soil is exported from the Site. Also, based on our experience working with the San Diego County Department of Health Services (DEH), it is recommended that soil that is classified as a hazardous waste be exported to an appropriately licensed facility rather than be left on-Site. • For “clean” or inert (Inert 2) soil that is exported from the Site, the San Diego RWQCB Tier 1 Soil Screening Levels 3 (SSLs) established in the RWQCB Order No. R9-2019-0005, Conditional Waivers of Waste Discharge Requirements for Low Threat Discharges in the San Diego Region, May 2019 (Waiver) are intended to be the criteria by which exported waste soil is judged to be inert, described within the Waiver as “inert waste soils that can be reused without restriction.” 2 Inert soil - For the purposes of this Report, Inert is defined as soil that does not contain detectable concentrations of constituents of concern with the possible exception of California Code Regulations Title 22 metals (with metals concentrations below the San Diego Regional Water Quality Control Board [RWQCB] Tier 1 Soil Screening Levels using a 90 percent upper confidence limit), or leachable concentrations of organic constituents that are consistent with the definition of “inert waste” specified in California Code of Regulations Title 27, section 20230, consistent with the RWQCB Order No. R9-2019-0005, Conditional Waivers of Waste Discharge Requirements for Low Threat Discharges in the San Diego Region, May 2019 (Waiver). This soil may consist of native/formational material as well as fill soil that does not have significant quantities of debris. 3 The Tier 1 SSLs presented in the RWQCB Waiver are intended to be the criteria by which soils are judged to be Inert waste soils that can be reused without restriction, subject to the General Waiver Conditions. The General Waiver Conditions stipulate that discharges/disposal of solid wastes to land must not be allowed to directly or indirectly enter any municipal separate storm sewer system (MS4s) or surface waters of the State, must not cause or threaten to cause a condition of contamination, pollution, or nuisance, and must comply with local, State, and federal ordinances and regulations and obtain any required permits, certifications, and/or licenses. Phase II ESA www.scsengineers.com 6 o For chemical CoCs including TPH, VOCs, and PAHs, all soil containing any detectable or leachable concentrations of chemical CoCs proposed for export off Site would need to be disposed of as regulated, non-hazardous waste at a minimum per the Tier 1 SSLs. o For metals that are naturally occurring, the Tier 1 SSL for lead is 23.9 milligrams per kilogram (mg/kg) and the Tier 1 SSL for arsenic is 3.5 mg/kg. If soil was to be exported as Inert, excavated Site soils must be shown through the collection of soil samples and analysis for lead and other metals, with the 90% upper confidence limit (UCL), to be below the Tier 1 SSL. • Non-hazardous regulated waste soils are exported soils that have concentrations of CoCs that exceed the Tier 1 SSLs (discussed above), and also have concentrations of CoCs below hazardous waste-based criteria (discussed below). Non-hazardous regulated soils must be disposed of at a properly licensed facility, such as a landfill. The acceptance of non- hazardous soils at disposal facilities are subject to the acceptance criteria established by these facilities. • For characterizing soil as hazardous waste, the California Code of Regulations, Title 22 Article 3, was used. o Soil is characterized as a California hazardous waste, at a minimum, upon exceedance of the total concentrations of a CoC to the Total Threshold Limit Concentration (TTLC), and/or by comparing the results of a Waste Extraction Test (WET) to the Soluble Threshold Limit Concentration (STLC). o Soil is characterized as a federal or Resource, Conservation, and Recovery Act (RCRA) hazardous waste through an exceedance of Toxicity Characteristic Leaching Procedure (TCLP) laboratory results upon comparison to the respective Maximum Contaminant Concentration for the Toxicity Characteristic (MCCTC). 4 FINDINGS TOPOGRAPHY, GEOLOGY, HYDROGEOLOGY, AND WATER QUALITY SURVEY Topography A topographic map for the Site vicinity was reviewed and is summarized in the following table. Reported Elevation 135 to 220 feet above mean sea level Reported Slope Direction Slopes down to the south toward the Otay River Source United States Geological Survey 7.5 Minute Topographic Map Imperial Beach Quadrangle, California – San Diego County, 2018 Phase II ESA www.scsengineers.com 7 Geology A geological map for the Site vicinity was reviewed and is summarized in the following table. Reported Formation Young alluvial flood plain deposits (Qya) Holocene and late Pleistocene aged Reported Description Poorly consolidated, poorly sorted, permeable flood-plain deposits of sandy, silty or clay-bearing alluvium Source Kennedy, Michael P., and Siang S. Tan, Geologic Map of the San Diego 30' × 60' Quadrangle, California, California Geological Survey, 2008 Hydrogeology Data regarding depth to groundwater and flow direction for the Site were not readily available. In the absence of Site-specific data, depth to groundwater and flow direction information was reviewed for properties within the Site vicinity using the State Water Resources Control Board GeoTracker database. The following table summarizes the results of this review. Property Location Approximately 425 feet to the west of the Site Reported Depth to Groundwater 48.3 feet below grade in monitoring well MW12, closest to the Site Reported Groundwater Flow Direction Southwest Source Second Semi-Annual 2020 Groundwater Monitoring and Remedial Progress Report Former Crown Chemical Corporation Facility, 1888 Nirvana Avenue Chula Vista, California 91911 prepared by Arcadis and dated January 29, 2021 Please note that many variables influence depth to groundwater and flow direction and the actual depth to groundwater and flow direction at the Site may be different than presented in this section. Water Quality Survey The following table summarizes the reported water quality in the Site vicinity. Reported Hydrologic Area Otay Valley (910.20) Reported Hydrologic Unit Otay (910.00) Reported Beneficial Use Industrial Source California RWQCB, San Diego Region, Water Quality Control Plan for the San Diego Basin, September 8, 1994, with amendments effective prior to May 17, 2016 Phase II ESA www.scsengineers.com 8 LABORATORY ANALYTICAL RESULTS AND SCREENING Soil Vapor Sample Analytical Results A summary of the laboratory analytical results for soil vapor is presented below. A complete listing of the results is presented in the laboratory analytical report included in Appendix A. The data are presented in Table 1 and depicted on Figure 2. VOCs A total of four soil vapor samples, identified as SV1-4, SV2-2, SV3-3, and SV3-3 Rep, were analyzed for VOCs in general accordance with EPA Method TO-15. Carbon disulfide was reported to be present in one of the four soil vapor samples at the concentration of 47 micrograms per liter (µg/L) (SV2-2). Toluene was reported to be present in three of the four soil vapor samples at concentrations ranging from 8.8 µg/L (SV3-3 Rep) and 19 µg/L (SV2-2). m,p-Xylene was reported to be present in two of the four soil vapor samples at concentrations ranging from 9.2 µg/L (SV3-3) and 26 µg/L (SV2-2). o-Xylene was reported to be present in one of the four soil vapor samples at the concentration of 7.2 µg/L (SV2-2). 1,2,4-Trimethlybenzene was reported to be present in one of the four soil vapor samples at the concentration of 12 µg/L (SV2-2). Chloroform was reported to be present in one of the four soil vapor samples at the concentration of 9.0 µg/L (SV1-4). All other VOCs analyzed were reported to be below the respective laboratory reporting limits. Please refer to the analytical laboratory reports contained in Appendix A for a full listing of VOCs analyzed and their respective reporting limits. Since VOCs were reported to be present above laboratory reporting limits, a vapor intrusion risk screening (VIRS) was conducted to assess the likelihood that a Significant vapor intrusion risk exists at the Site as a result of vapor phase migration of CVOCs. See the “Vapor Intrusion Risk Screening (VIRS)” section below. VOCs in Soil Vapor The VOCs reported to be present in soil vapor beneath the Site included carbon disulfide, toluene, m,p-xylene, o-xylene, 1,2,4-trimethylbenzene, and chloroform. Carbon disulfide, toluene, m,p-xylene, o-xylene, and 1,2,4-trimethylbenzene are typical constituents of petroleum hydrocarbons, likely from the nearby industrial properties or other off-Site sources. Chloroform is a routine drinking water disinfection byproduct (trihalomethanes) and is often present in soil and soil vapor from treated tap water via irrigation or other sources of drinking water. Chloroform is formed when chlorine reacts with natural organic humic materials and bromine via the haloform reaction in water.4 Overall, based on the low concentrations at which they were detected, it’s unlikely the VOCs in soil vapor resulted 4 Morrison, D. and B.L. Murphy. 2013. Chlorinated Solvents: A Forensic Evaluation. RSC Publishing. Cambridge. Phase II ESA www.scsengineers.com 9 from a point source or significant release at the Site, but more likely have migrated beneath the Site from the nearby industrial properties or another off-Site source. Vapor Intrusion Risk Screening (VIRS) Since VOCs were reported to be present in soil vapor beneath the Site, a VIRS was conducted to assess the potential for Significant human health risk posed to occupants of the proposed commercial/industrial Site buildings due to the upward migration of VOCs in soil vapor. SCS understands that as of January 24, 2019, the DTSC has archived the Johnson and Ettinger Human Health Risk Assessment Model. Therefore, SCS has conducted a vapor intrusion risk screening using current DTSC screening criteria, as described below, and the Site-specific slab attenuation factor, as described above. Approach VOCs may originate from either impacted soil or groundwater. In this case, VOCs are interpreted to be from possible subsurface impacts from the adjacent upgradient industrial facilities or another off- Site source, which were able to migrate in soil vapor beneath the Site. The highest soil vapor concentrations detected beneath the Site were conservatively assumed to be present beneath the entire Site to estimate conservative case-scenario-predicted indoor air concentrations for the future commercial/industrial buildings at the Site. The estimates of the theoretical indoor air concentrations were then compared against the most recently published screening levels 5 to assess the potential for Significant human health risk posed to commercial/industrial users of the Site due to the upward migration of VOCs in soil vapor. The VIRS was conducted using the DTSC default Attenuation Factor6 (AF) of 0.0005 for future commercial industrial buildings. To be conservative, the AF was applied to the highest reported concentration of each constituent (carbon disulfide, toluene, m,p-xylene, o-xylene, 1,2,4- trimethlybenzene, and chloroform) reported in soil vapor. The resulting values were compared against the DTSC-Modified Screening Levels (DTSC-SLs) provided in DTSC Human Health Risk Assessment (HHRA) Note 3.5 VIRS Results The maximum reported concentrations of VOCs detected at the Site are presented in the table below, along with the associated DTSC-SL. Please note that only the constituents reported to be present beneath the Site building were evaluated. VOC Maximum Concentration Detected Beneath the Site Building Predicted Indoor Air Concentration1 DTSC/EPA Screening Levels2 (µg/m3) Carbon disulfide 47 0.0235 3,100^ Toluene 19 0.0095 1,300 m,p-Xylene 26 0.013 440^ o-Xylene 7.2 0.0036 440^ 5 Human Health Risk Assessment Note 3 - DTSC-Modified Screening Levels (DTSC-SLs), Table 3. Screening Levels for Ambient Air, June 2020 Update. 6 Department of Toxic Substances Control (DTSC), State of California Vapor Intrusion Guidance Document - Final, dated October 2011. Phase II ESA www.scsengineers.com 10 VOC Maximum Concentration Detected Beneath the Site Building Predicted Indoor Air Concentration1 DTSC/EPA Screening Levels2 (µg/m3) 1,2,4- Trimethylbenzene 12 0.006 260^ Chloroform 9.0 0.0045 0.53^ Notes: µg/m3 – micrograms per cubic meter. 1 Soil vapor concentration multiplied by the attenuation factor (AF) of 0.0005 for future commercial use, as determined by DTSC Final Vapor Intrusion Guidance dated October 2011. 2 DTSC Human Health Risk Assessment Note 3 - DTSC-Modified Screening Levels (DTSC-SLs), June 2020. ^ A DTSC-SL has not been established for this constituent (carbon disulfide, m,p- and o-xylenes, and 1, 2, 4- trimethylbenzene). The Environmental Protection Agency (EPA) Regional Screening Level (RSL), dated November 2021, was used for this constituent. After applying the DTSC attenuation factor of 0.0005 for a future commercial/industrial land use to the maximum reported concentrations of the constituents reported to be present beneath the Site (carbon disulfide, toluene, m,p-xylene, o-xylene, 1,2,4-trimethylbenzene, and chloroform), the maximum theoretical concentrations of VOCs in indoor air at the Site are below the commercial/industrial screening levels (DTSC-SLs or RSLs).7 Soil Sample Analytical Results A summary of the laboratory analytical results for soil is presented below, along with screening the reported results to the Site to the Health Risk-Based Mitigation Criteria and Waste-Based Mitigation Criteria, as defined in the “Soil Screening Regulatory Criteria for CoC-Bearing Soil” section above. A complete listing of the results is presented in the laboratory analytical report included in Appendix A. The data are presented in Tables 1 through 3 and depicted on Figure 3. Lead and Other Metals Soil analytical results for lead and other metals are summarized here: 7 Note that vapor intrusion standards are currently in a state of transition, and if more conservative standards are adopted, it is possible that in using the vapor concentration data obtained by SCS that the derived theoretical indoor air concentrations exceed applicable indoor air screening criteria. For example, if a default attenuation factor of 0.03 for sub-slab soil vapor and “near-source” exterior soil vapor was used, as described in 2015 by USEPA and USEPA and in February 2020 by DTSC in their Draft Supplemental Guidance: Screening and Evaluating Vapor Intrusion, the reported maximum chloroform concentration at the Site exceed residential EPA screening level (U.S. Environmental Protection Agency Office of Solid Waste and Emergency Response (OSWER) June 2015 – OWSER Technical Guide for Assessing and Mitigating the Vapor Intrusion Pathway from Subsurface Vapor Sources to Indoor Air). However, the 2015 EPA Guidance indicates attenuation factors for deeper soil vapor data would be expected to be less than those for sub-slab soil vapor due to additional attenuation through the vadose zone. It is our understanding that, based on recent projects with DTSC oversight, the DTSC is still allowing the use of the DTSC 2011 Guidance and attenuation factors. Therefore, based on our experience and because this assessment includes deeper soil vapor sampling depths than sub-slab depths, the DTSC 2011 Guidance is used herein. Phase II ESA www.scsengineers.com 11 Title 22 Metal Number of Samples Analyzed Number of Detections Maximum Site Concentration (mg/kg) Waste-Based Screening Health Risk-Based Screening Tier 1 SSL (mg/kg) Above Tier 1 SSL? DTSC RSL/ EPA RSL (mg/kg) Above DTSC RSL/ EPA RSL? Lead 3 3 33.6 23.9 Yes 80 No Antimony 3 1 0.699 5.0 No 31 No Arsenic 3 3 5.10 3.5 Yes 12* No Barium 3 3 111 509 No 22,000 No Beryllium 3 0 <0.500 4.0 No 6,900 No Cadmium 3 3 1.43 4.0 No 4,000 No Chromium 3 3 16.9 122 No 1,800,000 No Cobalt 3 3 4.73 20 No 350 No Copper 3 3 25.3 60 No 47,000 No Mercury 3 0 <0.0500 0.26 No 4.4 No Molybdenum 3 2 1.69 2.0 No 5,800 No Nickel 3 3 7.77 57 No 64,000 No Selenium 3 0 <0.500 0.21 No 5,800 No Silver 3 0 <0.500 2.0 No 5,800 No Thallium 3 0 <0.500 0.78 No 1.2 No Vanadium 3 3 39.6 112 No 5,800 No Zinc 3 3 170 149 Yes 350,000 No Notes: mg/kg - milligrams per kilogram. Waste-Based Screening - Tier 1 SSLs = Tier 1 Soil Screening Level for inert waste soils that can be reused without restriction. For exceedances, the 90 percent upper confidence limit was used to derive a Site-specific value, as discussed in the Report below. Health Risk-Based Screening – DTSC RSL/ EPA RSL = Health Risk-Based Criteria - For metals, the DTSC HERO HHRA Note Number: 3, June 2020, using the RSLs for commercial/ industrial soil and cancer endpoint, or, for other metals not listed in HHRA Note 3, the Regional Screening levels for commercial/ industrial soil, provided by the EPA and updated as of May 2021 were used. < - Concentration reported below the listed laboratory reporting limit. * - For arsenic, although the DTSC RSL is 0.11 mg/kg, concentrations of naturally occurring arsenic typically exceed human health risk screening criteria. Therefore, the DTSC upper- bound background concentration for arsenic of 12 mg/kg was used. Red font – the maximum Site concentration for a particular metal exceeds the Tier 1 SSL. Comparison of Metals Concentrations to Waste-Based Mitigation Criteria (i.e., for Soil Export) The analytical results of the Title 22 metal analyses were compared to the respective Tier 1 SSL for each metal, which are established in the San Diego RWQCB Waiver2 and apply to waste export (i.e., for soil that is exported from the Site only). Tier 1 SSLs were exceeded in select sample results for lead, arsenic, and zinc. Below is a discussion of each metal that was reported with concentrations that exceed the Tier 1 SSL. Arsenic – Three soil samples were reported to exceed the Tier 1 SSL for arsenic (samples SB1, SB2, and SB3); they were collected from a depth of approximately 0.5 feet within the drainage channels and reported with arsenic concentrations of 5.10, 3.73, and 3.70 mg/kg, respectively. Phase II ESA www.scsengineers.com 12 Although arsenic was reported to exceed the DTSC RSL for commercial land use and select samples exceed the Tier 1 SSL for soil that is exported, the levels reported were within typical background concentration ranges. In an abstract presented by Department of Toxic Substances Control staff at the 2008 Society of Toxicology Annual Meeting,8 it was reported that the upper-bound background concentration for arsenic in southern California soil is 12 mg/kg. Therefore, the maximum reported arsenic concentration of 5.10 mg/kg is below the upper-bound background concentration of 12 mg/kg established by the DTSC. Therefore, the reported arsenic concentrations in shallow soil at the Site are within the range of typical background concentrations and do not appear to be indicative of a release of arsenic. Lead - One soil sample was reported to exceed the Tier 1 SSL for lead (sample SB1); it was collected from the depth of approximately 0.5 feet within the southern portion of the western drainage channel and reported with a lead concentration of 33.6 mg/kg. The Client reported that it is not known whether soil export will be required during the grading activities for the proposed project. If soil export is proposed for the Site, it is recommended that the soil proposed for export be tested for lead so that the soil can be characterized for proper disposal. Zinc - One soil sample was reported to exceed the Tier 1 SSL for zinc (sample SB1); it was collected from the depth of approximately 0.5 feet within the southern portion of the western drainage channel and reported with a zinc concentration of 170 mg/kg. The Client reported that it is not known whether soil export will be required during the grading activities for the proposed project. If soil export is proposed for the Site, it is recommended that the soil proposed for export be tested for zinc so that the soil can be characterized for proper disposal. Comparison of Metals Concentrations to Risk-Based Mitigation Criteria (i.e., for Soil that Remains on-Site) Regarding the comparison of metals to Risk-Based Mitigation Criteria, with the exception of arsenic, the reported metals concentrations are below applicable residential human health risk-screening criteria (i.e., DTSC HERO HHRA Note Number 3, June 2020, and EPA RSLs, May 2021). For the metal arsenic, concentrations were reported above the DTSC RSL for arsenic of 0.36 mg/kg in all three of the soil samples analyzed for arsenic. Although arsenic was reported to exceed the commercial/industrial DTSC RSL, the levels reported were below the DTSC upper-bound background concentration for arsenic in southern California soil of 12 mg/kg. Therefore, the maximum reported arsenic concentration of 5.10 mg/kg is below the upper-bound background concentration of 12 mg/kg established by the DTSC. Therefore, the reported arsenic concentrations in shallow soil at the Site are within the range of typical background concentrations and do not appear to be indicative of a release of arsenic. Total Petroleum Hydrocarbons (TPH) Soil analytical results for TPH were compared to Waste Based Mitigation-Criteria (i.e., Tier 1 SSLs) and Health Risk-Based Mitigation Criteria (i.e., SFBRWQCB ESLs) as summarized in the table below. 8 Determination of a Southern California Regional Background Arsenic Concentration in Soil, Chernoff, G., Bosan, W., Oudiz, D., and California Department of Toxic Substances Control, 2008 Society of Toxicology Annual Meeting. Phase II ESA www.scsengineers.com 13 Analyte Maximum Site Concentration (mg/kg) Waste-Based Screening1 Health Risk-Based Screening1 Tier 1 SSL (mg/kg) Above Tier 1 SSL? Mitigation Criteria (mg/kg) Above Mitigation Criteria? TPHg <0.5 ND No 2,000 No TPHd 128 ND Yes 1,200 No TPHo 352 ND Yes 180,000 No Notes: mg/kg = milligrams per kilogram. 1= Waste-Based Screening - Tier 1 SSLs = Tier 1 Soil Screening Level for inert waste soils that can be reused without restriction. 2= Health Risk-Based Mitigation Criteria - San Francisco Bay Regional Water Quality Control Board (SFBRWQCB), Environmental Screening Levels for commercial/industrial users (ESLs) (2019, Rev. 2). Risk value was not established; the non-cancer hazard value was used. TPHg= TPH as gasoline. TPHd= TPH as diesel. TPHo= TPH as oil. <= Not detected above the specified laboratory reporting limit. Red font = the maximum Site concentration for a particular metal exceeds the waste-based screening criteria or health risk-based screening criteria. Comparison of TPH Concentrations to Waste-Based Mitigation Criteria (i.e., for Soil Export) Regarding waste-based screening criteria, detectable concentrations of chemical constituents such as TPH would be considered a regulated waste if exported from the Site per the RWQCB Tier 1 SSLs. A total of five of the eight soil samples (samples SB1, SB2, SB4-0.5, SB7-0.5, and SB8-0.5) analyzed for TPH were reported with detectable concentrations of TPH; soil represented by these samples would be considered a regulated waste if exported from the Site. The Client reported that it is not known whether soil export will be required during the grading activities for the proposed project. If soil export is proposed for the Site, it is recommended that the soil proposed for export be tested for TPH so that the soil can be characterized for proper disposal. Comparison of TPH Concentrations to Risk-Based Mitigation Criteria (i.e., for Soil that Remains on-Site) TPH was not detected above the Health Risk-Based Mitigation in any of the eight soil samples collected and analyzed. Therefore, based on the soil samples collected and analyzed for TPH, the soil is not considered to represent a human health risk to future commercial/industrial users of the Site, and can be freely graded on-Site during proposed grading activities. Volatile Organic Compounds (VOCs) The eight soil samples analyzed for VOCs were reported to be below the respective laboratory reporting limits. Please refer to the analytical laboratory reports contained in Appendix A for a full listing of VOCs analyzed and their respective reporting limits. Phase II ESA www.scsengineers.com 14 Polycyclic Aromatic Hydrocarbons (PAHs) The PAHs benzo(a)anthracene, chrysene, fluoranthene, phenanthrene, and were reported above the laboratory reporting limits in various samples collected and analyzed from the Site. Below is a discussion of the reported concentrations of PAHs at the Site compared to soil screening regulatory criteria. PAHs Maximum Site Concentration Waste-Based Screening1 Health Risk-Based Screening3 Tier 1 SSL Abov e Tier 1 SSL? SFBRWQCB ESL/ DTSC RSL/ EPA RSL Above SFBRWQCB ESL/ DTSC RSL/ EPA RSL? µg/kg Benzo(a)anthracene 10.7 ND Yes 12,000 No Chrysene 15.3 ND Yes 1,300,000 No Fluoranthene 22.7 ND Yes 18,000,000 No Phenanthrene 14.7 ND Yes NE No Pyrene 19.3 ND Yes 13,000,000 No Notes: µg/kg: micrograms per kilogram. 1) Waste-Based Screening - Tier 1 SSLs = Tier 1 Soil Screening Level for inert waste soils that can be reused without restriction. 2) Hazardous Waste Criteria: Values shown from CA code of regulations, Title 22 Article 3, July 20, 2005, regarding characteristics of hazardous waste. Exceedances of the TTLC would be considered a California hazardous waste, at a minimum. 3) Health Risk-Based Criteria - For PAHs based on DTSC HERO HHRA Note Number: 3, June 2020, using the Recommended Screening Levels for industrial/commercial soil, or, for chemicals not listed in HHRA Note 3, the Regional Screening levels for residential soil, provided by the EPA and updated as of May 2021 were used. * = Health risk- and hazardous waste-based criteria for alpha chlordane not available; therefore, applicable criteria from chlordane used. ND = non-detect above the specified laboratory reporting limits. Red font = the maximum Site concentration for a particular metal exceeds the waste-based screening criteria or health risk-based screening criteria. Comparison of PAH Concentrations to Waste-Based Mitigation Criteria (i.e., for Soil Export) Regarding waste-based screening criteria, detectable concentrations of chemical constituents such as PAH would be considered a regulated waste if exported from the Site per the RWQCB Tier 1 SSLs. A total of three of the five soil samples (samples SB4-0.5, SB7-0.5, and SB8-0.5) analyzed for PAHs were reported with detectable concentrations of PAHs; soil represented by these samples would be considered a regulated waste if exported from the Site. The Client reported that it is not known whether soil export will be required during the grading activities for the proposed project. If soil export is proposed for the Site, it is recommended that the soil proposed for export be tested for PAH so that the soil can be characterized for proper disposal. Phase II ESA www.scsengineers.com 15 Comparison of PAH Concentrations to Risk-Based Mitigation Criteria (i.e., for Soil that Remains on-Site) PAHs were not detected above the Health Risk-Based Mitigation in any of the five soil samples collected and analyzed. Therefore, based on the soil samples collected and analyzed for PAHs, the soil is not considered to represent a human health risk to future commercial/industrial users of the Site, and can be freely graded on-Site during grading activities. 5 CONCLUSIONS Based on the samples collected as part of this Phase II Environmental Site Assessment (ESA), laboratory results, current regulatory guidelines, and SCS’ experience and professional judgment, SCS concludes and recommends the following: Background • SCS performed a Phase II ESA consisting of the following: o Advancement and sampling of three soil vapor probes (identified as SV1 through SV3), and the collection of four soil vapor samples (including a replicate sample) from depths ranging 2 to 4 feet below grade for analysis of volatile organic compounds (VOCs), in order to assess possible impacts from the northern adjacent industrial properties, and from some former totes previously situated adjacent to the northeastern portion of the Site. Note that sample depths of 5 feet deep could not be attained due to practical refusal encountered with a hand held roto-hammer, the only sampling method considered feasible for the steep and rugged terrain at the Site. o Advancement of three soil borings using a trowel (borings SB1 through SB3) and five soil borings by using a hand-held auger (borings SB4 through SB8) to total depths of up to 2.0 feet below grade at the Site to assess the possible presence and concentrations of constituents of concern (CoCs) (i.e., petroleum hydrocarbons, Title 22 metals, polycyclic aromatic hydrocarbons [PAHs], and volatile organic compounds [VOCs]) within representative locations within the on-Site drainage channels, in connection with possible impacts from the northern adjacent industrial properties. Soil Vapor Investigation • The VOCs carbon disulfide, toluene, m,p-xylene, o-xylene, 1,2,4-trimethylbenzene, and chloroform were reported to be present in soil vapor beneath the Site. o Carbon disulfide, toluene, m,p-xylene, o-xylene, and 1,2,4-trimethylbenzene are typical constituents of petroleum hydrocarbons, likely from the nearby industrial facilities or another off-Site source. Chloroform is a routine drinking water disinfection byproduct (trihalomethanes) and is often present in soil and soil vapor from treated tap water via irrigation or other sources of drinking water. o Overall, based on the low concentrations at which they were detected, it’s unlikely the VOCs in soil vapor resulted from a point source or significant release at the Site, but more likely have migrated beneath the Site from the nearby industrial facilities facility or another off-Site source. Phase II ESA www.scsengineers.com 16 • Because VOCs were reported above the laboratory reporting limits in the soil vapor samples collected from the Site, a vapor intrusion risk screening (VIRS) was conducted to assess the potential for Significant vapor intrusion risk posed to the future commercial/industrial occupants at the Site due to the upward migration of VOCs in soil vapor. o After applying the Department of Toxic Substances Control (DTSC) attenuation factor 0.0005 for a future commercial/industrial land use to the maximum reported concentrations of the constituents reported to be present beneath the Site (carbon disulfide, toluene, m,p-xylene, o-xylene, 1,2,4-trimethylbenzene, and chloroform), the maximum theoretical concentrations of VOCs in indoor air at the Site are below the commercial/industrial screening levels (DTSC- Modified Screening Levels or EPA Regional Screening Levels). Soil Investigation • Detectable concentrations of total petroleum hydrocarbons (TPH) and Polycyclic Aromatic Hydrocarbons (PAHs) and somewhat elevated concentrations of the metals arsenic, lead, and zinc were reported to be present in certain samples collected at the Site and exceed Waste-Based Mitigation Criteria (i.e., Regional Water Quality Control Board [RWQCB] Tier 1 Soil Screening Levels [SSLs]). Reported concentrations of TPH include relatively low concentrations in the diesel and oil carbon chain lengths. Reported concentrations of PAHs include relatively low concentrations of benzo(a)anthracene, chrysene, fluoranthene, phenanthrene, and pyrene, and would be considered a regulated waste, likely a non- hazardous regulated waste, if this soil is exported from the Site. In the event that the soil is exported from the Site, representative portions of the stockpiles to be exported should be analyzed for TPH, Title 22 metals, and PAHs for proper waste characterization and disposal. • With the possible exception of arsenic that is further described in the bullet below, none of the reported TPH, PAHs, and metal concentrations were reported to exceed Health Risk- Based Mitigation Criteria for commercial/industrial users established by the DTSC (Recommended Screening Levels [RSLs]), San Francisco Bay Regional Water Quality Control Board (Environmental Screening Levels), and US Environmental Protection Agency (RSLs), as stipulated in the Report. Therefore, based on the soil samples collected and analyzed for TPH, PAHs, VOCs, and Title 22 metals, the soil is not considered to represent a human health risk to future commercial/industrial users of the Site, and can be freely graded on-Site during grading activities. • For the metal arsenic, concentrations were reported above the DTSC RSL for arsenic of 0.36 milligrams per kilogram (mg/kg) in all three of the soil samples analyzed for arsenic. Arsenic was reported with a maximum concentration of 5.10 mg/kg at the Site. Although arsenic concentrations at the Site reported to exceed the commercial/industrial DTSC RSL and the Tier 1 SSL for arsenic, the levels reported were below the DTSC upper-bound background concentration for arsenic in southern California soil of 12 mg/kg. Therefore, the maximum reported arsenic concentration of 5.10 mg/kg is below the upper-bound background concentration of 12 mg/kg established by the DTSC. Therefore, the reported arsenic concentrations in shallow soil at the Site are within the range of typical background concentrations and do not appear to be indicative of a release of arsenic. Phase II ESA www.scsengineers.com 17 6 RECOMMENDATIONS Based on the data obtained during this Assessment and our conclusions, current regulatory guidelines, and our experience and professional judgment, SCS recommends the following: Soil Vapor Investigation • No further action for the Site related to soil vapor intrusion at this time for the proposed commercial/industrial land use. Soil Investigation • The Client reported that it is not known whether soil import will be required during the grading activities for the proposed project. If soil export is proposed for the Site, it is recommended that the soil proposed for export be tested for the identified CoCs for the Site including TPH, PAHs, and Title 22 metals and so that the soil can be characterized for proper disposal. 7 REPORT USAGE AND FUTURE SITE CONDITIONS This Report is intended for the sole usage of the Client and other parties designated by SCS. The methodology used during this Phase II ESA was in general conformance with the requirements of the Client and the specifications and limitations presented in the Master Services Agreement (Contract) between the Client and SCS. This Report contains information from a variety of public and other sources, and SCS makes no representation or warranty about the accuracy, reliability, suitability, or completeness of the information. Any use of this Report, whether by the Client or by a third party, shall be subject to the provisions of the Contract between the Client and SCS. Any misuse of or reliance upon the Report shall be without risk or liability to SCS. Assessments are qualitative, not comprehensive, in nature and may not identify all environmental problems or eliminate all risk. For every property, but especially for properties in older downtown or urban areas, it is possible for there to be unknown, unreported recognized environmental conditions, USTs, or other features of concern that might become apparent through demolition, construction, or excavation activities, etc. In addition, the scope of services for this project was limited to those items specifically named in the scope of services for this Report. Environmental issues not specifically addressed in the scope of services for this project are not included in this Report. Land use, condition of the properties within the Site, and other factors may change over time. The information and conclusions of this Report are judged to have been relevant at the time the work described in this Report was conducted. This Report should not be relied upon to represent future Site conditions unless a qualified consultant familiar with the practice of Phase II Environmental Site Assessments in the County of San Diego is consulted to assess the necessity of updating this Report. The property owners at the Site are solely responsible for notifying all governmental agencies and the public of the existence, release, or disposal of any hazardous materials/wastes or petroleum products at the Site, whether before, during, or after the performance of SCS’ services. SCS assumes no responsibility or liability for any claim, loss of property value, damage, or injury that results from hazardous materials/wastes or petroleum products being present or encountered within the Site. Although this Phase II ESA has attempted to assess the likelihood that the Site has been impacted by a hazardous material/waste release, potential sources of impact may have escaped detection for Phase II ESA www.scsengineers.com 18 reasons that include, but are not limited to, (1) inadequate or inaccurate information rightfully provided to SCS by third parties, such as public agencies and other outside sources; (2) the limited scope of this Phase II ESA; and (3) the presence of undetected, unknown, or unreported environmental releases. 7 LIKELIHOOD STATEMENTS Statements of “likelihood” have been made in this report. Likelihood statements are based on professional judgments of SCS. The term “likelihood,” as used herein, pertains to the probability of a match between the prediction for an event and its actual occurrence. The likelihood statement assigns a measure for a “degree of belief” for the match between the prediction for the event and the actual occurrence of the event. The likelihood statements in this Report are made qualitatively (expressed in words). The qualitative terms can be approximately related to quantitative percentages. The term “low likelihood” is used by SCS to approximate a range of 10 to 20 percent; the term “moderate likelihood” refers to an approximate range of 40 to 60 percent; and the term “high likelihood” refers to an approximate range of 80 to 90 percent. 8 SPECIAL CONTRACTUAL CONDITIONS BETWEEN USER AND ENVIRONMENTAL PROFESSIONAL There were no special contractual conditions between the user of this Phase II ESA, the environmental professional, and SCS. Phase II ESA www.scsengineers.com Tables Table 1 Soil Vapor Sample Analytical Results 821 Main Street Chula Vista, California Carbon Disulfide Toluene m,p-Xylene o-Xylene 1, 2, 4- Trimethlybenzene Chloroform Other VOCs SV1-4 4 11/11/2021 < 6.3 < 3.8 < 8.8 < 4.4 < 5.0 9.0 ND SV2-2 2 11/11/2021 47 19 26 7.2 12 < 4.9 ND SV3-3 3 11/11/2021 < 6.3 9.8 9.2 < 4.4 < 5.0 < 4.9 ND SV3-3 Rep 3 11/11/2021 < 6.3 8.8 < 8.8 < 4.4 < 5.0 < 4.9 ND 47 19 26 7.2 12 9.0 0.0235 0.0095 0.013 0.0036 0.006 0.0045 3,100^1,300 440^440^260^0.53^ Notes: < = less than indicated laboratory reporting limit. ND = group of constituents not detected above laboratory reporting limits; refer to the laboratory analytical report for a full listing of analytes and associated reporting limits. Bold = analyte detected above laboratory reporting limit. Results presented in micrograms per cubic meter (µg/m3). 1= Maximum soil vapor concentration multiplied by the default Department of Substances Control (DTSC) attenuation factor of 0.0005 for a future commercial building, per Table 2 - Attenuation Factors for Preliminary Screening Evaluations of the Vapor Intrusion Guidance. 2= Human Health Risk Assessment Note 3 - DTSC-Modified Screening Levels (DTSC-SLs), Table 3 - Screening Levels for Ambient Air, Commercial/Industrial June 2020 update. ^ A DTSC-SL has not been established for this constituent (carbon disulfide, m,p- and o-xylenes, and 1, 2, 4-trimethylbenzene). The Environmental Protection Agency (EPA) Regional Screening Level (RSL), dated May 2021, was used for this constituent. ug/m3 Sample Identifier Depth (feet bgs)Date Collected Maximum Site Concentration (µg/m3) Predicted Indoor Air Concentration for Future Commercial Use1 Commercial DTSC/EPA Screening Level2 (µg/m3) Soil vapor samples collected by SCS Engineers on November 11, 2021, and analyzed for volatile organic compounds (VOCs) in accordance with EPA Method TO-15. Depth in feet below ground surface (bgs). Table 2 Soil Sample Analytical Results for TPH, VOCs, and PAHs 821 Main Street Chula Vista, California Benzo(a)anthracene Chrysene Fluoranthene Phenanthrene Pyrene All other PAHs SB1 0.5 7/13/2021 210 74.0 < 0.500 ND -- -- -- -- -- -- SB2 0.5 7/13/2021 290 74.0 < 0.500 ND -- -- -- -- -- -- SB3 0.5 7/13/2021 < 50.0 < 10.0 < 0.500 ND -- -- -- -- -- -- SB4-0.5 0.5 11/11/21 82.4 < 10.0 < 0.500 ND 4.00 15.3 9.33 < 5.80 10.0 ND SB5-0.5 0.5 11/11/2021 < 50.0 < 10.0 < 0.500 ND < 5.0 < 5.0 < 5.0 < 5.0 < 5.0 ND SB6-0.5 0.5 11/11/2021 < 50.0 < 10.0 < 0.500 ND < 5.0 < 5.0 < 5.0 < 5.0 < 5.0 ND SB7-0.5 0.5 11/11/2021 352 128 < 0.500 ND 4.67 10.0 10.0 < 5.80 10.7 ND SB8-0.5 0.5 11/11/2021 298 58.0 < 0.500 ND 10.7 15.3 22.7 14.7 19.3 ND 180,000 1,200 2,000 NA 12,000 1,300,000 18,000,000 ^7,800 13,000,000 NA Notes: Soil samples collected by SCS Engineers on 7/13/21 and 11/11/21. VOCs: Volatile Organic Compounds. Samples from SCS analyzed in general accordance with EPA Method 8260B. TPH: Total Petroleum Hydrocarbons. Samples from SCS analyzed in general accordance with EPA Method 8015B. Polycyclic Aromatic Hydrocarbons (PAHs) samples analyzed in general accordance with EPA Method 8270C. mg/kg : milligrams per kilogram. µg/kg : micrograms per kilogram. < : less than the laboratory reporting limit. bgs : below ground surface ND: Not detected above the laboratory reporting limit. TPHo: TPH oil-range organics. TPHd: TPH diesel-range organics. TPHg: TPH gasoline-range organics. -- : not analyzed. ND : not detected above the laboratory reporting limits for the group of constituents. 1) Health Risk-Based Criteria - For TPH, VOCs the San Francisco Bay Regional Water Quality Control Board (SFBRWQCB) Environmental Screening Levels (ESLs) for commercial/ industrial users, dated 2019 (revised). For PAHs the Department of Toxic Substances Control (DTSC) Human and Ecological Risk Office (HERO) Human Health Risk Assessment (HHRA) Note Number: 3, June 2020, using the recommended Screening Levels (SL) for industrial soil. ^For chemicals not listed in HHRA Note 3, the EPA RSLs for commercial/industrial soil, November 2021 were used. NA: Not applicable. Bold : Result indicating above laboratory reporting limits. Health Risk-Based Criteria 1 mg/kg µg/kg Sample Depth in Feet bgs Date TPHo TPHd TPHg VOCs PAHs Table 3 Soil Sample Analytical Results for Metals 821 Main Street Chula Vista, California Lead Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Mercury Molybdenu m Nickel Selenium Silver Thallium Vanadiu m Zinc SB1 0.5 7/13/2021 33.6 0.699 5.10 111 < 0.500 1.43 16.9 4.73 22.5 < 0.0500 1.00 7.77 < 0.500 < 0.500 < 0.500 39.6 170 SB2 0.5 7/13/2021 7.99 < 0.500 3.73 55.0 < 0.500 1.13 12.7 4.61 25.3 < 0.0500 1.69 5.20 < 0.500 < 0.500 < 0.500 35.3 58.1 SB3 0.5 7/13/2021 7.33 < 0.500 3.70 110 < 0.500 0.863 5.79 3.82 5.87 < 0.0500 < 0.500 3.13 < 0.500 < 0.500 < 0.500 26.7 33.8 80 31 12 22,000 6,900 4,000 1,800,000 350 47,000 4.4 5,800 64,000 5,800 5,800 1.2 5,800 350,000 1,000 500 500 10,000 75 100 2,500 8,000 2,500 20 3,500 2,000 100 500 700 2,400 5,000 Notes: Soil samples collected by SCS Engineers on 7/13/21. Soil samples were analyzed for Title 22 metals by Environmental Protection Agency (EPA) Method 6010B. mg/kg : milligrams per kilogram. < : less than the laboratory reporting limit. bgs : below ground surface Bold : Result indicating above laboratory reporting limits. 1) Health Risk-Based Criteria - For lead, the Department of Toxic Substances Control (DTSC) Human and Ecological Risk Office (HERO) Human Health Risk Assessment (HHRA) Note Number: 3, June 2020, using the Recommended Screening Levels (RSL) for commercial/ industrial soil and cancer endpoint, or, for other metals not listed in HHRA Note 3, the Regional Screening levels for commercial/industrial soil, provided by the EPA and updated as of November 2021 were used. For arsenic, although the DTSC RSL is 0.11 mg/kg, naturally occuring arsenic typically exceeds human health risk screening criteria. Therefore, the DTSC upper-bound background concentration for arsenic of 12 mg/kg was used. 2) Hazardous Waste Criteria: Values shown from CA code of regulations, Title 22 Article 3, July 20, 2005 regarding characteristics of hazardous waste. Exceedances of the Total Threshold Limit Concentration (TTLC) would be considered a California hazardous waste, at a minimum. Hazardous Waste Criteria2 Sample Depth in Feet bgs Date mg/kg Health Risk-Based Criteria1 Phase II ESA www.scsengineers.com Figures North (Not to scale) Disclaimer: This figure is based on available data. Actual conditions may differ. All locations and dimensions are approximate. FOUR-WAY SITE LOCATION MAP VWP-OP Nirvana Owner, LLC 821 Main Street Chula Vista, California Reference: U.S.G.S. 7.5 Minute Quadrangle Map Imperial Beach, California Reference: U.S.G.S. 7.5 Minute Quadrangle Map Imperial Beach, California Reference: Google Earth Aerial Photograph Chula Vista, California - December 2020 REGIONAL SITE LOCATION 2-DIMENSIONAL SITE LOCATION 3-DIMENSIONAL SITE LOCATIONSITE AERIAL PHOTOGRAPH North (Not to scale) North (Not to scale) North (Not to scale) SANTA YSABEL North IslandNAS S a n D i e g o B a y MissionBayMissionBayMissionBay BONSALLBONSALLBONSALL LAKESIDE SAN DIEGO EL CAJON LA MESA FALLBROOK PALA ESCONDIDO SANTEE ALPINE CARLSBAD LEUCADIA ENCINITAS DEL MAR LA JOLLA SOLANA BEACH CARDIFF-BY-THE-SEA TECATE VISTA SAN MARCOS JULIAN DEHESA Camp Pendleton (U.S.M.C.) FallbrookNaval Weapons Station MCAS Miramar Forest Cleveland National Forest Anza-Borrego Desert Anza-Borrego Desert TIJUANA California Mexico Lake Henshaw Lake Sutherland Lake Hodges El Capitan Lake Loveland Reservoir CorteMadero Lake Barrett Lake Lake Morena Lake MurrayLake MurrayLake Murray Lower Otay Lake SweetwaterReservoir Lake Jennings San VicenteLake Lake Wohlford Lake Poway DixonLake Cleveland National JACUMBA CAMPO VALLEY CENTERVALLEY CENTERVALLEY CENTEROCEANSIDE RAMONA PINE VALLEY MISSION BEACH PACIFIC BEACH OCEAN BEACH CORONADO IMPERIAL BEACH BORREGO SPRINGS WARNER SPRINGS 94 67 54 54 94 78 7878 76 79 POWAY 79 Cuyamaca Rancho State Park LEMON GROVELEMON GROVELEMON GROVE JAMUL ToLos Angeles ToPalm Springs To San Bernardinoand Las Vegas 79 371 DESCANSO SPRINGVALLEYSPRINGVALLEYSPRINGVALLEY TEMECULA S.D. Int'l Airport(Lindbergh Field) Brown FieldMun. Airport PalomarAirport OceansideMun. Airport Montgomery Field Airport SAN YSIDRO ToIndio ToEl Centro ToEl Centro 8 8 5 5 76 78 1 5 805 15 15 15 15 125 163 905 Balboa Park 5 805 NATIONALCITYNATIONALCITYNATIONALCITY Riverside County San Diego County Im p e r i a l C o u n t y Sa n D i e g o C o u n t y Orange County 5 94 94 52 CHULAVISTACHULAVISTACHULAVISTA Figure 1 Project No.: 01221156.00 Date Drafted: 9/15/21 OTAY MESA BONITABONITABONITA MIRA MESAMIRA MESAMIRA MESA S C S E N G I N E E R S Environmental Consultants 8799 Balboa Avenue, Suite 290 San Diego, California 92123 P A C I F I C O C E A N 56 Project Site Project Site Project Site Project Site Disclaimer: This figure is based on available data. Actual conditions may differ. All locations and dimensions are approximate. S C S E N G I N E E R S Environmental Consultants 8799 Balboa Avenue, Suite 290 San Diego, California 92123 Figure 2 Project No.: 01221156.00 Date Drafted: 12/7/21 LEGEND Approximate Site boundary Trash/debris pile Approximate soil sample location Approximate soil vapor sample location Approximate location of drainages Reference: Google Earth Aerial Photograph Chula Vista, California - December 2020 0 60 120 180 Approximate Graphic Scale in Feet 1 inch = 120 feet North SV2 2’ 47 19 26 7.2 12 <4.9 ND Depth CD Toluene m,p-Xylene o-Xylene 1,2,4-TMB CF Other VOCs Soil vapor samples, with depth in feet below grade, collected by SCS Engineers on November 11, 2021, and analyzed for volatile organic compounds (VOCs) by EPA Method TO-15. Results reported in micrograms per cubic meter (μg/m3). Bold font indicates sample results above the laboratory reporting limit. < indicates results less than the laboratory reporting limit; number indicates individual analyte reporting limit. ND indicates concentration not detected above laboratory reporting limits. CD = carbon disulfide CF = chloroform 1,2,4-TMB = 1,2,4-trimethylbenzene APN 644-050-07 (Vacant Land) APN 644-050-07 (Vacant Land) APN 644-050-07 (Vacant Land) APN 644-050-10 (Vacant Land) APN 644-050-10 (Vacant Land) APN 644-050-10 (Vacant Land) APN 644-050-14APN 644-050-14APN 644-050-14 Western Portion of APN 644-050-08 Western Portion of APN 644-050-08 Western Portion of APN 644-050-08 APN 644-050-13APN 644-050-13APN 644-050-13 821 Main Street Vacant Land (Site) 821 Main Street Vacant Land (Site) 821 Main Street Vacant Land (Site) SB3SB3SB3 SB1SB1SB1 SB2SB2SB2 SB8SB8SB8 SB4SB4SB4 SB5SB5SB5 SB6SB6SB6 SB7SB7SB7 Former tote system Former tote system Former tote system SV1 4’ <6.3 <3.8 <8.8 <4.4 <5.0 9.0 ND Depth CD Toluene m,p-Xylene o-Xylene 1,2,4-TMB CF Other VOCs SV2 2’ 47 19 26 7.2 12 <4.9 ND Depth CD Toluene m,p-Xylene o-Xylene 1,2,4-TMB CF Other VOCs SV3/SV3 Rep 3’ <6.3 9.8 9.2 <4.4 <5.0 <4.9 ND 3’ <6.3 8.8 <8.8 <4.4 <5.0 <4.9 ND Depth CD Toluene m,p-Xylene o-Xylene 1,2,4-TMB CF Other VOCs SITE PLAN WITH SOIL VAPORANALYTICAL RESULTSVWP-OP Nirvana Owner, LLC 821 Main Street Chula Vista, California Disclaimer: This figure is based on available data. Actual conditions may differ. All locations and dimensions are approximate. S C S E N G I N E E R S Environmental Consultants 8799 Balboa Avenue, Suite 290 San Diego, California 92123 Figure 3 Project No.: 01221156.00 Date Drafted: 12/7/21 LEGEND Approximate Site boundary Trash/debris pile Approximate soil sample location Approximate soil vapor sample location Approximate location of drainages Reference: Google Earth Aerial Photograph Chula Vista, California - December 2020 0 60 120 180 Approximate Graphic Scale in Feet 1 inch = 120 feet North Soil samples, with depth in feet below grade, collected by SCS Engineers on July 13 and November 11, 2021, and analyzed for total petroleum hydrocarbons as gasoline, diesel, and oil (TPHg, TPHd, TPHo, respectively) by EPA Method 8015B, Title 22 Metals by EPA Method 6010B, volatile organic compounds (VOCs) by EPA Method 8260B, and polynuclear aromatic hydrocarbons (PAHs) by EPA Method 8270C. Results for TPH and Title 22 Metals reported in milligrams per kilogram (mg/kg). Results for VOCs and PAHs reported in micrograms per kilogram (μg/kg). Bold font indicates sample results above the laboratory reporting limit. < indicates results less than the laboratory reporting limit; number indicates individual analyte reporting limit. ND indicates not detected above laboratory reporting limits. NA indicates not analyzed. Pb = Lead Sb = Antimony As = Arsenic Ba = Barium Cd = Cadmium Cr = Chromium Co = Cobalt Cu = Copper Mo = Molybdenum Ni = Nickel V = Vanadium Zn = Zinc APN 644-050-07 (Vacant Land) APN 644-050-07 (Vacant Land) APN 644-050-07 (Vacant Land) APN 644-050-10 (Vacant Land) APN 644-050-10 (Vacant Land) APN 644-050-10 (Vacant Land) APN 644-050-14APN 644-050-14APN 644-050-14 Western Portion of APN 644-050-08 Western Portion of APN 644-050-08 Western Portion of APN 644-050-08 APN 644-050-13APN 644-050-13APN 644-050-13 821 Main Street Vacant Land (Site) 821 Main Street Vacant Land (Site) 821 Main Street Vacant Land (Site) SV1SV1SV1 SV2SV2SV2 SV3SV3SV3 Former tote system Former tote system Former tote system SB4 0.5’ <0.5 <10 82.4 ND 4.00 15.3 9.33 <5.8 10.0 ND Depth TPHg TPHd TPHo VOCs Benzo(a)anthracene Chrysene Fluoranthene Phenanthrene Pyrene Other PAHs SB5 0.5’ <0.5 <10 <50 ND <5.0 <5.0 <5.0 <5.0 <5.0 ND Depth TPHg TPHd TPHo VOCs Benzo(a)anthracene Chrysene Fluoranthene Phenanthrene Pyrene Other PAHs SB6 0.5’ <0.5 <10 <50 ND <5.0 <5.0 <5.0 <5.0 <5.0 ND Depth TPHg TPHd TPHo VOCs Benzo(a)anthracene Chrysene Fluoranthene Phenanthrene Pyrene Other PAHs SB7 0.5’ <0.5 128 352 ND 4.67 10.0 10.0 <5.8 10.7 ND Depth TPHg TPHd TPHo VOCs Benzo(a)anthracene Chrysene Fluoranthene Phenanthrene Pyrene Other PAHs SB8 0.5’ <0.5 58.0 298 ND 10.7 15.3 22.7 14.7 19.3 ND Depth TPHg TPHd TPHo VOCs Benzo(a)anthracene Chrysene Fluoranthene Phenanthrene Pyrene Other PAHs SB1 0.5’ <0.5 74.0 210 33.6 0.699 5.10 111 1.43 16.9 4.73 22.5 1.00 7.77 39.6 170 ND ND NA Depth TPHg TPHd TPHo Pb Sb As Ba Cd Cr Co Cu Mo Ni V Zn Other Metals VOCs PAHs SB1 0.5’ <0.5 74.0 210 33.6 0.699 5.10 111 1.43 16.9 4.73 22.5 1.00 7.77 39.6 170 ND ND NA Depth TPHg TPHd TPHo Pb Sb As Ba Cd Cr Co Cu Mo Ni V Zn Other Metals VOCs PAHs SB3 0.5’ <0.5 <10 <50 7.33 3.70 110 0.863 5.79 3.82 5.87 3.13 26.7 33.8 ND ND NA Depth TPHg TPHd TPHo Pb As Ba Cd Cr Co Cu Ni V Zn Other Metals VOCs PAHs SB2 0.5’ <0.5 74.0 290 7.99 3.73 55.0 1.13 12.7 4.61 25.3 1.69 5.20 35.3 58.1 ND ND NA Depth TPHg TPHd TPHo Pb As Ba Cd Cr Co Cu Mo Ni V Zn Other Metals VOCs PAHs SITE PLAN WITH SOIL SAMPLE ANALYTICAL RESULTS VWP-OP Nirvana Owner, LLC 821 Main Street Chula Vista, California Phase II ESA www.scsengineers.com Appendix A Laboratory Analytical Reports SCS Engineers Project Name: Nirvana Properties San Diego, CA 92123 8799 Balboa Avenue, Suite 290 Luke Montague Enclosed are the results of analyses for samples received by the laboratory on November 11, 2021. If you have any questions concerning this report, please feel free to contact us. 17 November 2021 Project ID: 01221156.00 Site Address: 821 Main Street Chula Vista, CA American Scientific Laboratories, LLC (ASL) accepts sample materials from clients for analysis with the assumption that all of the information provided to ASL verbally or in writing by our clients (and/or their agents), regarding samples being submitted to ASL, is complete and accurate. ASL accepts all samples subject to the following conditions: 1) ASL is not responsible for verifying any client -provided information regarding any samples submitted to the laboratory. 2) ASL is not responsible for any consequences resulting from any inaccuracies , omissions, or misrepresentations contained in client-provided information regarding samples submitted to the laboratory. Work Order #: 2111096 Laboratory Director Molky Brar Page 1 of 28 Page 2 of 28 Page 3 of 28 Page 4 of 28 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 01221156.00 Luke Montague Nirvana Properties 11/17/2021 12:58San Diego CA, 92123 2111096Work Order No: ANALYTICAL SUMMARY REPORT Sample ID Laboratory ID Matrix Date Sampled Date Received SB8-0.5 2111096-01 Solid 11/11/2021 08:47 11/11/2021 14:00 SB7-0.5 2111096-04 Solid 11/11/2021 09:04 11/11/2021 14:00 SB4-0.5 2111096-07 Solid 11/11/2021 09:43 11/11/2021 14:00 SB5-0.5 2111096-10 Solid 11/11/2021 10:04 11/11/2021 14:00 SB6-0.5 2111096-13 Solid 11/11/2021 10:27 11/11/2021 14:00 Amolk Brar, Lab Director The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Page 3 of 26Page 5 of 28 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 01221156.00 Luke Montague Nirvana Properties 11/17/2021 12:58San Diego CA, 92123 2111096Work Order No: ResultAnalyte PQL Analyzed MethodNotes DilutionUnits Laboratory Sample ID: 2111096-01 (Solid) Prep Method Analyst Client Sample ID: SB8-0.5 Analytical Results MDL Total Petroleum Hydrocarbons(TPH-g)Batch ID:BK10608 Prepared:11/11/2021 17:00 ND 11/12/2021 15:19Gasoline Range Organics 500 ug/kg 1 8015B5030ADW250 11/12/2021 15:1970-120103 %Surrogate: Bromofluorobenzene 8015B5030ADW Total Petroleum Hydrocarbons(TPH DROORO)Batch ID:BK10606 Prepared:11/12/2021 10:00 58.0 11/13/2021 02:57Diesel range organics 20.0 mg/kg 2 8015B3550BDW2.00 298 11/13/2021 02:57Oil Range Organics 100 mg/kg 2 8015B3550BDW34.0 11/13/2021 02:5770-120100 %Surrogate: Chlorobenzene 8015B3550BDW Volatile Organic Compounds Batch ID:BK10607 Prepared:11/11/2021 17:00 ND 11/12/2021 13:05Acetone50.0 ug/kg 1 8260B5030ADW12.7 ND 11/12/2021 13:05Benzene2.00 ug/kg 1 8260B5030ADW0.930 ND 11/12/2021 13:05Bromobenzene10.0 ug/kg 1 8260B5030ADW3.39 ND 11/12/2021 13:05Bromochloromethane10.0 ug/kg 1 8260B5030ADW0.380 ND 11/12/2021 13:05Bromodichloromethane10.0 ug/kg 1 8260B5030ADW0.630 ND 11/12/2021 13:05Bromoform50.0 ug/kg 1 8260B5030ADW3.39 ND 11/12/2021 13:05Bromomethane30.0 ug/kg 1 8260B5030ADW2.75 ND 11/12/2021 13:052-Butanone 50.0 ug/kg 1 8260B5030ADW5.83 ND 11/12/2021 13:05n-Butylbenzene 10.0 ug/kg 1 8260B5030ADW2.05 ND 11/12/2021 13:05sec-Butylbenzene 10.0 ug/kg 1 8260B5030ADW3.04 ND 11/12/2021 13:05tert-Butylbenzene 10.0 ug/kg 1 8260B5030ADW1.34 ND 11/12/2021 13:05Carbon disulfide 10.0 ug/kg 1 8260B5030ADW5.53 ND 11/12/2021 13:05Carbon tetrachloride 10.0 ug/kg 1 8260B5030ADW2.48 ND 11/12/2021 13:05Chlorobenzene10.0 ug/kg 1 8260B5030ADW0.890 ND 11/12/2021 13:05Chloroethane30.0 ug/kg 1 8260B5030ADW2.15 ND 11/12/2021 13:052-Chloroethylvinyl Ether 50.0 ug/kg 1 8260B5030ADW5.53 ND 11/12/2021 13:05Chloroform10.0 ug/kg 1 8260B5030ADW1.24 ND 11/12/2021 13:05Chloromethane30.0 ug/kg 1 8260B5030ADW1.74 ND 11/12/2021 13:054-Chlorotoluene 10.0 ug/kg 1 8260B5030ADW1.34 ND 11/12/2021 13:052-Chlorotoluene 10.0 ug/kg 1 8260B5030ADW2.35 ND 11/12/2021 13:051,2-Dibromo-3-chloropropane 50.0 ug/kg 1 8260B5030ADW2.69 ND 11/12/2021 13:05Dibromochloromethane10.0 ug/kg 1 8260B5030ADW0.650 ND 11/12/2021 13:051,2-Dibromoethane 10.0 ug/kg 1 8260B5030ADW2.75 ND 11/12/2021 13:05Dibromomethane10.0 ug/kg 1 8260B5030ADW2.30 ND 11/12/2021 13:051,2-Dichlorobenzene 10.0 ug/kg 1 8260B5030ADW1.65 ND 11/12/2021 13:051,3-Dichlorobenzene 10.0 ug/kg 1 8260B5030ADW1.03 ND 11/12/2021 13:051,4-Dichlorobenzene 10.0 ug/kg 1 8260B5030ADW2.23 Amolk Brar, Lab Director The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Page 4 of 26Page 6 of 28 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 01221156.00 Luke Montague Nirvana Properties 11/17/2021 12:58San Diego CA, 92123 2111096Work Order No: ResultAnalyte PQL Analyzed MethodNotes DilutionUnits Laboratory Sample ID: 2111096-01 (Solid) Prep Method Analyst Client Sample ID: SB8-0.5 Analytical Results MDL Volatile Organic Compounds Batch ID:BK10607 Prepared:11/11/2021 17:00 ND 11/12/2021 13:05Dichlorodifluoromethane30.0 ug/kg 1 8260B5030ADW2.07 ND 11/12/2021 13:051,1-Dichloroethane 10.0 ug/kg 1 8260B5030ADW1.30 ND 11/12/2021 13:051,2-Dichloroethane 10.0 ug/kg 1 8260B5030ADW1.57 ND 11/12/2021 13:051,1-Dichloroethene 10.0 ug/kg 1 8260B5030ADW1.60 ND 11/12/2021 13:05cis-1,2-Dichloroethene 10.0 ug/kg 1 8260B5030ADW2.16 ND 11/12/2021 13:05trans-1,2-Dichloroethene 10.0 ug/kg 1 8260B5030ADW2.60 ND 11/12/2021 13:051,1-Dichloropropene 10.0 ug/kg 1 8260B5030ADW0.660 ND 11/12/2021 13:051,2-Dichloropropane 10.0 ug/kg 1 8260B5030ADW0.920 ND 11/12/2021 13:051,3-Dichloropropane 10.0 ug/kg 1 8260B5030ADW1.36 ND 11/12/2021 13:052,2-Dichloropropane 10.0 ug/kg 1 8260B5030ADW1.12 ND 11/12/2021 13:05cis-1,3-Dichloropropene 10.0 ug/kg 1 8260B5030ADW0.980 ND 11/12/2021 13:05trans-1,3-Dichloropropene 10.0 ug/kg 1 8260B5030ADW0.960 ND 11/12/2021 13:05Ethylbenzene2.00 ug/kg 1 8260B5030ADW1.00 ND 11/12/2021 13:05Hexachlorobutadiene30.0 ug/kg 1 8260B5030ADW2.77 ND 11/12/2021 13:052-Hexanone 50.0 ug/kg 1 8260B5030ADW3.18 ND 11/12/2021 13:05Isopropylbenzene10.0 ug/kg 1 8260B5030ADW1.42 ND 11/12/2021 13:05p-Isopropyltoluene 10.0 ug/kg 1 8260B5030ADW3.86 ND 11/12/2021 13:05Methyl tert-Butyl Ether (MTBE)5.00 ug/kg 1 8260B5030ADW1.81 ND 11/12/2021 13:054-Methyl-2-pentanone (MIBK)50.0 ug/kg 1 8260B5030ADW3.14 ND 11/12/2021 13:05Methylene chloride 50.0 ug/kg 1 8260B5030ADW3.31 ND 11/12/2021 13:05Naphthalene10.0 ug/kg 1 8260B5030ADW1.14 ND 11/12/2021 13:05n-Propylbenzene 10.0 ug/kg 1 8260B5030ADW1.14 ND 11/12/2021 13:05Styrene10.0 ug/kg 1 8260B5030ADW0.800 ND 11/12/2021 13:051,1,1,2-Tetrachloroethane 10.0 ug/kg 1 8260B5030ADW1.28 ND 11/12/2021 13:051,1,2,2-Tetrachloroethane 10.0 ug/kg 1 8260B5030ADW3.25 ND 11/12/2021 13:05Tetrachloroethene10.0 ug/kg 1 8260B5030ADW0.930 ND 11/12/2021 13:05Toluene2.00 ug/kg 1 8260B5030ADW1.00 ND 11/12/2021 13:051,2,3-Trichlorobenzene 10.0 ug/kg 1 8260B5030ADW1.23 ND 11/12/2021 13:051,2,4-Trichlorobenzene 10.0 ug/kg 1 8260B5030ADW2.82 ND 11/12/2021 13:051,1,1-Trichloroethane 10.0 ug/kg 1 8260B5030ADW2.03 ND 11/12/2021 13:051,1,2-Trichloroethane 10.0 ug/kg 1 8260B5030ADW1.74 ND 11/12/2021 13:05Trichloroethene10.0 ug/kg 1 8260B5030ADW1.15 ND 11/12/2021 13:05Trichlorofluoromethane10.0 ug/kg 1 8260B5030ADW3.15 ND 11/12/2021 13:051,2,3-Trichloropropane 10.0 ug/kg 1 8260B5030ADW1.74 ND 11/12/2021 13:051,2,4-Trimethylbenzene 10.0 ug/kg 1 8260B5030ADW3.19 ND 11/12/2021 13:051,3,5- Trimethylbenzene 10.0 ug/kg 1 8260B5030ADW1.23 Amolk Brar, Lab Director The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Page 5 of 26Page 7 of 28 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 01221156.00 Luke Montague Nirvana Properties 11/17/2021 12:58San Diego CA, 92123 2111096Work Order No: ResultAnalyte PQL Analyzed MethodNotes DilutionUnits Laboratory Sample ID: 2111096-01 (Solid) Prep Method Analyst Client Sample ID: SB8-0.5 Analytical Results MDL Volatile Organic Compounds Batch ID:BK10607 Prepared:11/11/2021 17:00 ND 11/12/2021 13:05Vinyl acetate 50.0 ug/kg 1 8260B5030ADW10.8 ND 11/12/2021 13:05Vinyl chloride 30.0 ug/kg 1 8260B5030ADW2.79 ND 11/12/2021 13:05m,p-Xylenes 4.00 ug/kg 1 8260B5030ADW1.80 ND 11/12/2021 13:05o-Xylene 2.00 ug/kg 1 8260B5030ADW1.00 11/12/2021 13:0570-12090.1 %Surrogate: 4-Bromofluorobenzene 8260B5030ADW 11/12/2021 13:0570-12075.0 %Surrogate: Dibromofluoromethane 8260B5030ADW 11/12/2021 13:0570-12089.8 %Surrogate: Toluene-d8 8260B5030ADW 8270 PAH SIM Batch ID:BK10609 Prepared:11/15/2021 09:10 ND 11/15/2021 16:12Acenaphthene20.0 ug/kg 4 8270C3550 SV AY5.52 ND 11/15/2021 16:12Acenaphthylene20.0 ug/kg 4 8270C3550 SV AY5.52 ND 11/15/2021 16:12Anthracene20.0 ug/kg 4 8270C3550 SV AY4.96 10.7 11/15/2021 16:12Benzo(a)anthracene 20.0J ug/kg 4 8270C3550 SV AY3.40 ND 11/15/2021 16:12Benzo[a]pyrene 20.0 ug/kg 4 8270C3550 SV AY9.20 ND 11/15/2021 16:12Benzo[b]fluoranthene 20.0 ug/kg 4 8270C3550 SV AY9.24 ND 11/15/2021 16:12Benzo(ghi)perylene 20.0 ug/kg 4 8270C3550 SV AY20.0 ND 11/15/2021 16:12Benzo[k]fluoranthene 20.0 ug/kg 4 8270C3550 SV AY9.72 15.3 11/15/2021 16:12Chrysene20.0J ug/kg 4 8270C3550 SV AY5.68 ND 11/15/2021 16:12Dibenz(a,h)anthracene 20.0 ug/kg 4 8270C3550 SV AY18.9 22.7 11/15/2021 16:12Fluoranthene20.0 ug/kg 4 8270C3550 SV AY4.16 ND 11/15/2021 16:12Fluorene20.0 ug/kg 4 8270C3550 SV AY5.00 ND 11/15/2021 16:12Indeno (1,2,3-cd) pyrene 20.0 ug/kg 4 8270C3550 SV AY17.7 ND 11/15/2021 16:12Naphthalene20.0 ug/kg 4 8270C3550 SV AY6.32 14.7 11/15/2021 16:12Phenanthrene20.0J ug/kg 4 8270C3550 SV AY5.80 19.3 11/15/2021 16:12Pyrene20.0J ug/kg 4 8270C3550 SV AY4.12 11/15/2021 16:1235-11471.6 %Surrogate: Nitrobenzene-d5 8270C3550 SV AY 11/15/2021 16:1221-10530.4 %Surrogate: 1,4-Dioxane-d8 8270C3550 SV AY ResultAnalyte PQL Analyzed MethodNotes DilutionUnits Laboratory Sample ID: 2111096-04 (Solid) Prep Method Analyst Client Sample ID: SB7-0.5 Analytical Results MDL Total Petroleum Hydrocarbons(TPH-g)Batch ID:BK10608 Prepared:11/11/2021 17:00 ND 11/12/2021 15:48Gasoline Range Organics 500 ug/kg 1 8015B5030ADW250 Amolk Brar, Lab Director The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Page 6 of 26Page 8 of 28 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 01221156.00 Luke Montague Nirvana Properties 11/17/2021 12:58San Diego CA, 92123 2111096Work Order No: ResultAnalyte PQL Analyzed MethodNotes DilutionUnits Laboratory Sample ID: 2111096-04 (Solid) Prep Method Analyst Client Sample ID: SB7-0.5 Analytical Results MDL Total Petroleum Hydrocarbons(TPH-g)Batch ID:BK10608 Prepared:11/11/2021 17:00 11/12/2021 15:4870-120109 %Surrogate: Bromofluorobenzene 8015B5030ADW Total Petroleum Hydrocarbons(TPH DROORO)Batch ID:BK10606 Prepared:11/12/2021 10:00 128 11/13/2021 03:40Diesel range organics 20.0 mg/kg 2 8015B3550BDW2.00 352 11/13/2021 03:40Oil Range Organics 100 mg/kg 2 8015B3550BDW34.0 11/13/2021 03:4070-120102 %Surrogate: Chlorobenzene 8015B3550BDW Volatile Organic Compounds Batch ID:BK10607 Prepared:11/11/2021 17:00 ND 11/12/2021 13:31Acetone50.0 ug/kg 1 8260B5030ADW12.7 ND 11/12/2021 13:31Benzene2.00 ug/kg 1 8260B5030ADW0.930 ND 11/12/2021 13:31Bromobenzene10.0 ug/kg 1 8260B5030ADW3.39 ND 11/12/2021 13:31Bromochloromethane10.0 ug/kg 1 8260B5030ADW0.380 ND 11/12/2021 13:31Bromodichloromethane10.0 ug/kg 1 8260B5030ADW0.630 ND 11/12/2021 13:31Bromoform50.0 ug/kg 1 8260B5030ADW3.39 ND 11/12/2021 13:31Bromomethane30.0 ug/kg 1 8260B5030ADW2.75 ND 11/12/2021 13:312-Butanone 50.0 ug/kg 1 8260B5030ADW5.83 ND 11/12/2021 13:31n-Butylbenzene 10.0 ug/kg 1 8260B5030ADW2.05 ND 11/12/2021 13:31sec-Butylbenzene 10.0 ug/kg 1 8260B5030ADW3.04 ND 11/12/2021 13:31tert-Butylbenzene 10.0 ug/kg 1 8260B5030ADW1.34 ND 11/12/2021 13:31Carbon disulfide 10.0 ug/kg 1 8260B5030ADW5.53 ND 11/12/2021 13:31Carbon tetrachloride 10.0 ug/kg 1 8260B5030ADW2.48 ND 11/12/2021 13:31Chlorobenzene10.0 ug/kg 1 8260B5030ADW0.890 ND 11/12/2021 13:31Chloroethane30.0 ug/kg 1 8260B5030ADW2.15 ND 11/12/2021 13:312-Chloroethylvinyl Ether 50.0 ug/kg 1 8260B5030ADW5.53 ND 11/12/2021 13:31Chloroform10.0 ug/kg 1 8260B5030ADW1.24 ND 11/12/2021 13:31Chloromethane30.0 ug/kg 1 8260B5030ADW1.74 ND 11/12/2021 13:314-Chlorotoluene 10.0 ug/kg 1 8260B5030ADW1.34 ND 11/12/2021 13:312-Chlorotoluene 10.0 ug/kg 1 8260B5030ADW2.35 ND 11/12/2021 13:311,2-Dibromo-3-chloropropane 50.0 ug/kg 1 8260B5030ADW2.69 ND 11/12/2021 13:31Dibromochloromethane10.0 ug/kg 1 8260B5030ADW0.650 ND 11/12/2021 13:311,2-Dibromoethane 10.0 ug/kg 1 8260B5030ADW2.75 ND 11/12/2021 13:31Dibromomethane10.0 ug/kg 1 8260B5030ADW2.30 ND 11/12/2021 13:311,2-Dichlorobenzene 10.0 ug/kg 1 8260B5030ADW1.65 ND 11/12/2021 13:311,3-Dichlorobenzene 10.0 ug/kg 1 8260B5030ADW1.03 ND 11/12/2021 13:311,4-Dichlorobenzene 10.0 ug/kg 1 8260B5030ADW2.23 ND 11/12/2021 13:31Dichlorodifluoromethane30.0 ug/kg 1 8260B5030ADW2.07 Amolk Brar, Lab Director The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Page 7 of 26Page 9 of 28 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 01221156.00 Luke Montague Nirvana Properties 11/17/2021 12:58San Diego CA, 92123 2111096Work Order No: ResultAnalyte PQL Analyzed MethodNotes DilutionUnits Laboratory Sample ID: 2111096-04 (Solid) Prep Method Analyst Client Sample ID: SB7-0.5 Analytical Results MDL Volatile Organic Compounds Batch ID:BK10607 Prepared:11/11/2021 17:00 ND 11/12/2021 13:311,1-Dichloroethane 10.0 ug/kg 1 8260B5030ADW1.30 ND 11/12/2021 13:311,2-Dichloroethane 10.0 ug/kg 1 8260B5030ADW1.57 ND 11/12/2021 13:311,1-Dichloroethene 10.0 ug/kg 1 8260B5030ADW1.60 ND 11/12/2021 13:31cis-1,2-Dichloroethene 10.0 ug/kg 1 8260B5030ADW2.16 ND 11/12/2021 13:31trans-1,2-Dichloroethene 10.0 ug/kg 1 8260B5030ADW2.60 ND 11/12/2021 13:311,1-Dichloropropene 10.0 ug/kg 1 8260B5030ADW0.660 ND 11/12/2021 13:311,2-Dichloropropane 10.0 ug/kg 1 8260B5030ADW0.920 ND 11/12/2021 13:311,3-Dichloropropane 10.0 ug/kg 1 8260B5030ADW1.36 ND 11/12/2021 13:312,2-Dichloropropane 10.0 ug/kg 1 8260B5030ADW1.12 ND 11/12/2021 13:31cis-1,3-Dichloropropene 10.0 ug/kg 1 8260B5030ADW0.980 ND 11/12/2021 13:31trans-1,3-Dichloropropene 10.0 ug/kg 1 8260B5030ADW0.960 ND 11/12/2021 13:31Ethylbenzene2.00 ug/kg 1 8260B5030ADW1.00 ND 11/12/2021 13:31Hexachlorobutadiene30.0 ug/kg 1 8260B5030ADW2.77 ND 11/12/2021 13:312-Hexanone 50.0 ug/kg 1 8260B5030ADW3.18 ND 11/12/2021 13:31Isopropylbenzene10.0 ug/kg 1 8260B5030ADW1.42 ND 11/12/2021 13:31p-Isopropyltoluene 10.0 ug/kg 1 8260B5030ADW3.86 ND 11/12/2021 13:31Methyl tert-Butyl Ether (MTBE)5.00 ug/kg 1 8260B5030ADW1.81 ND 11/12/2021 13:314-Methyl-2-pentanone (MIBK)50.0 ug/kg 1 8260B5030ADW3.14 ND 11/12/2021 13:31Methylene chloride 50.0 ug/kg 1 8260B5030ADW3.31 ND 11/12/2021 13:31Naphthalene10.0 ug/kg 1 8260B5030ADW1.14 ND 11/12/2021 13:31n-Propylbenzene 10.0 ug/kg 1 8260B5030ADW1.14 ND 11/12/2021 13:31Styrene10.0 ug/kg 1 8260B5030ADW0.800 ND 11/12/2021 13:311,1,1,2-Tetrachloroethane 10.0 ug/kg 1 8260B5030ADW1.28 ND 11/12/2021 13:311,1,2,2-Tetrachloroethane 10.0 ug/kg 1 8260B5030ADW3.25 ND 11/12/2021 13:31Tetrachloroethene10.0 ug/kg 1 8260B5030ADW0.930 ND 11/12/2021 13:31Toluene2.00 ug/kg 1 8260B5030ADW1.00 ND 11/12/2021 13:311,2,3-Trichlorobenzene 10.0 ug/kg 1 8260B5030ADW1.23 ND 11/12/2021 13:311,2,4-Trichlorobenzene 10.0 ug/kg 1 8260B5030ADW2.82 ND 11/12/2021 13:311,1,1-Trichloroethane 10.0 ug/kg 1 8260B5030ADW2.03 ND 11/12/2021 13:311,1,2-Trichloroethane 10.0 ug/kg 1 8260B5030ADW1.74 ND 11/12/2021 13:31Trichloroethene10.0 ug/kg 1 8260B5030ADW1.15 ND 11/12/2021 13:31Trichlorofluoromethane10.0 ug/kg 1 8260B5030ADW3.15 ND 11/12/2021 13:311,2,3-Trichloropropane 10.0 ug/kg 1 8260B5030ADW1.74 ND 11/12/2021 13:311,2,4-Trimethylbenzene 10.0 ug/kg 1 8260B5030ADW3.19 ND 11/12/2021 13:311,3,5- Trimethylbenzene 10.0 ug/kg 1 8260B5030ADW1.23 ND 11/12/2021 13:31Vinyl acetate 50.0 ug/kg 1 8260B5030ADW10.8 Amolk Brar, Lab Director The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Page 8 of 26Page 10 of 28 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 01221156.00 Luke Montague Nirvana Properties 11/17/2021 12:58San Diego CA, 92123 2111096Work Order No: ResultAnalyte PQL Analyzed MethodNotes DilutionUnits Laboratory Sample ID: 2111096-04 (Solid) Prep Method Analyst Client Sample ID: SB7-0.5 Analytical Results MDL Volatile Organic Compounds Batch ID:BK10607 Prepared:11/11/2021 17:00 ND 11/12/2021 13:31Vinyl chloride 30.0 ug/kg 1 8260B5030ADW2.79 ND 11/12/2021 13:31m,p-Xylenes 4.00 ug/kg 1 8260B5030ADW1.80 ND 11/12/2021 13:31o-Xylene 2.00 ug/kg 1 8260B5030ADW1.00 11/12/2021 13:3170-12091.7 %Surrogate: 4-Bromofluorobenzene 8260B5030ADW 11/12/2021 13:3170-12074.6 %Surrogate: Dibromofluoromethane 8260B5030ADW 11/12/2021 13:3170-12093.6 %Surrogate: Toluene-d8 8260B5030ADW 8270 PAH SIM Batch ID:BK10609 Prepared:11/15/2021 09:10 ND 11/15/2021 16:42Acenaphthene20.0 ug/kg 4 8270C3550 SV AY5.52 ND 11/15/2021 16:42Acenaphthylene20.0 ug/kg 4 8270C3550 SV AY5.52 ND 11/15/2021 16:42Anthracene20.0 ug/kg 4 8270C3550 SV AY4.96 4.67 11/15/2021 16:42Benzo(a)anthracene 20.0J ug/kg 4 8270C3550 SV AY3.40 ND 11/15/2021 16:42Benzo[a]pyrene 20.0 ug/kg 4 8270C3550 SV AY9.20 ND 11/15/2021 16:42Benzo[b]fluoranthene 20.0 ug/kg 4 8270C3550 SV AY9.24 ND 11/15/2021 16:42Benzo(ghi)perylene 20.0 ug/kg 4 8270C3550 SV AY20.0 ND 11/15/2021 16:42Benzo[k]fluoranthene 20.0 ug/kg 4 8270C3550 SV AY9.72 10.0 11/15/2021 16:42Chrysene20.0J ug/kg 4 8270C3550 SV AY5.68 ND 11/15/2021 16:42Dibenz(a,h)anthracene 20.0 ug/kg 4 8270C3550 SV AY18.9 10.0 11/15/2021 16:42Fluoranthene20.0J ug/kg 4 8270C3550 SV AY4.16 ND 11/15/2021 16:42Fluorene20.0 ug/kg 4 8270C3550 SV AY5.00 ND 11/15/2021 16:42Indeno (1,2,3-cd) pyrene 20.0 ug/kg 4 8270C3550 SV AY17.7 ND 11/15/2021 16:42Naphthalene20.0 ug/kg 4 8270C3550 SV AY6.32 ND 11/15/2021 16:42Phenanthrene20.0 ug/kg 4 8270C3550 SV AY5.80 10.7 11/15/2021 16:42Pyrene20.0J ug/kg 4 8270C3550 SV AY4.12 11/15/2021 16:4235-11492.8 %Surrogate: Nitrobenzene-d5 8270C3550 SV AY 11/15/2021 16:4221-10527.2 %Surrogate: 1,4-Dioxane-d8 8270C3550 SV AY ResultAnalyte PQL Analyzed MethodNotes DilutionUnits Laboratory Sample ID: 2111096-07 (Solid) Prep Method Analyst Client Sample ID: SB4-0.5 Analytical Results MDL Total Petroleum Hydrocarbons(TPH-g)Batch ID:BK10608 Prepared:11/11/2021 17:00 ND 11/12/2021 16:17Gasoline Range Organics 500 ug/kg 1 8015B5030ADW250 11/12/2021 16:1770-120106 %Surrogate: Bromofluorobenzene 8015B5030ADW Amolk Brar, Lab Director The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Page 9 of 26Page 11 of 28 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 01221156.00 Luke Montague Nirvana Properties 11/17/2021 12:58San Diego CA, 92123 2111096Work Order No: ResultAnalyte PQL Analyzed MethodNotes DilutionUnits Laboratory Sample ID: 2111096-07 (Solid) Prep Method Analyst Client Sample ID: SB4-0.5 Analytical Results MDL Total Petroleum Hydrocarbons(TPH DROORO)Batch ID:BK10606 Prepared:11/12/2021 10:00 ND 11/13/2021 02:15Diesel range organics 10.0 mg/kg 1 8015B3550BDW1.00 82.4 11/13/2021 02:15Oil Range Organics 50.0 mg/kg 1 8015B3550BDW17.0 11/13/2021 02:1570-12099.2 %Surrogate: Chlorobenzene 8015B3550BDW Volatile Organic Compounds Batch ID:BK10607 Prepared:11/11/2021 17:00 ND 11/12/2021 13:57Acetone50.0 ug/kg 1 8260B5030ADW12.7 ND 11/12/2021 13:57Benzene2.00 ug/kg 1 8260B5030ADW0.930 ND 11/12/2021 13:57Bromobenzene10.0 ug/kg 1 8260B5030ADW3.39 ND 11/12/2021 13:57Bromochloromethane10.0 ug/kg 1 8260B5030ADW0.380 ND 11/12/2021 13:57Bromodichloromethane10.0 ug/kg 1 8260B5030ADW0.630 ND 11/12/2021 13:57Bromoform50.0 ug/kg 1 8260B5030ADW3.39 ND 11/12/2021 13:57Bromomethane30.0 ug/kg 1 8260B5030ADW2.75 ND 11/12/2021 13:572-Butanone 50.0 ug/kg 1 8260B5030ADW5.83 ND 11/12/2021 13:57n-Butylbenzene 10.0 ug/kg 1 8260B5030ADW2.05 ND 11/12/2021 13:57sec-Butylbenzene 10.0 ug/kg 1 8260B5030ADW3.04 ND 11/12/2021 13:57tert-Butylbenzene 10.0 ug/kg 1 8260B5030ADW1.34 ND 11/12/2021 13:57Carbon disulfide 10.0 ug/kg 1 8260B5030ADW5.53 ND 11/12/2021 13:57Carbon tetrachloride 10.0 ug/kg 1 8260B5030ADW2.48 ND 11/12/2021 13:57Chlorobenzene10.0 ug/kg 1 8260B5030ADW0.890 ND 11/12/2021 13:57Chloroethane30.0 ug/kg 1 8260B5030ADW2.15 ND 11/12/2021 13:572-Chloroethylvinyl Ether 50.0 ug/kg 1 8260B5030ADW5.53 ND 11/12/2021 13:57Chloroform10.0 ug/kg 1 8260B5030ADW1.24 ND 11/12/2021 13:57Chloromethane30.0 ug/kg 1 8260B5030ADW1.74 ND 11/12/2021 13:574-Chlorotoluene 10.0 ug/kg 1 8260B5030ADW1.34 ND 11/12/2021 13:572-Chlorotoluene 10.0 ug/kg 1 8260B5030ADW2.35 ND 11/12/2021 13:571,2-Dibromo-3-chloropropane 50.0 ug/kg 1 8260B5030ADW2.69 ND 11/12/2021 13:57Dibromochloromethane10.0 ug/kg 1 8260B5030ADW0.650 ND 11/12/2021 13:571,2-Dibromoethane 10.0 ug/kg 1 8260B5030ADW2.75 ND 11/12/2021 13:57Dibromomethane10.0 ug/kg 1 8260B5030ADW2.30 ND 11/12/2021 13:571,2-Dichlorobenzene 10.0 ug/kg 1 8260B5030ADW1.65 ND 11/12/2021 13:571,3-Dichlorobenzene 10.0 ug/kg 1 8260B5030ADW1.03 ND 11/12/2021 13:571,4-Dichlorobenzene 10.0 ug/kg 1 8260B5030ADW2.23 ND 11/12/2021 13:57Dichlorodifluoromethane30.0 ug/kg 1 8260B5030ADW2.07 ND 11/12/2021 13:571,1-Dichloroethane 10.0 ug/kg 1 8260B5030ADW1.30 ND 11/12/2021 13:571,2-Dichloroethane 10.0 ug/kg 1 8260B5030ADW1.57 ND 11/12/2021 13:571,1-Dichloroethene 10.0 ug/kg 1 8260B5030ADW1.60 Amolk Brar, Lab Director The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Page 10 of 26Page 12 of 28 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 01221156.00 Luke Montague Nirvana Properties 11/17/2021 12:58San Diego CA, 92123 2111096Work Order No: ResultAnalyte PQL Analyzed MethodNotes DilutionUnits Laboratory Sample ID: 2111096-07 (Solid) Prep Method Analyst Client Sample ID: SB4-0.5 Analytical Results MDL Volatile Organic Compounds Batch ID:BK10607 Prepared:11/11/2021 17:00 ND 11/12/2021 13:57cis-1,2-Dichloroethene 10.0 ug/kg 1 8260B5030ADW2.16 ND 11/12/2021 13:57trans-1,2-Dichloroethene 10.0 ug/kg 1 8260B5030ADW2.60 ND 11/12/2021 13:571,1-Dichloropropene 10.0 ug/kg 1 8260B5030ADW0.660 ND 11/12/2021 13:571,2-Dichloropropane 10.0 ug/kg 1 8260B5030ADW0.920 ND 11/12/2021 13:571,3-Dichloropropane 10.0 ug/kg 1 8260B5030ADW1.36 ND 11/12/2021 13:572,2-Dichloropropane 10.0 ug/kg 1 8260B5030ADW1.12 ND 11/12/2021 13:57cis-1,3-Dichloropropene 10.0 ug/kg 1 8260B5030ADW0.980 ND 11/12/2021 13:57trans-1,3-Dichloropropene 10.0 ug/kg 1 8260B5030ADW0.960 ND 11/12/2021 13:57Ethylbenzene2.00 ug/kg 1 8260B5030ADW1.00 ND 11/12/2021 13:57Hexachlorobutadiene30.0 ug/kg 1 8260B5030ADW2.77 ND 11/12/2021 13:572-Hexanone 50.0 ug/kg 1 8260B5030ADW3.18 ND 11/12/2021 13:57Isopropylbenzene10.0 ug/kg 1 8260B5030ADW1.42 ND 11/12/2021 13:57p-Isopropyltoluene 10.0 ug/kg 1 8260B5030ADW3.86 ND 11/12/2021 13:57Methyl tert-Butyl Ether (MTBE)5.00 ug/kg 1 8260B5030ADW1.81 ND 11/12/2021 13:574-Methyl-2-pentanone (MIBK)50.0 ug/kg 1 8260B5030ADW3.14 ND 11/12/2021 13:57Methylene chloride 50.0 ug/kg 1 8260B5030ADW3.31 ND 11/12/2021 13:57Naphthalene10.0 ug/kg 1 8260B5030ADW1.14 ND 11/12/2021 13:57n-Propylbenzene 10.0 ug/kg 1 8260B5030ADW1.14 ND 11/12/2021 13:57Styrene10.0 ug/kg 1 8260B5030ADW0.800 ND 11/12/2021 13:571,1,1,2-Tetrachloroethane 10.0 ug/kg 1 8260B5030ADW1.28 ND 11/12/2021 13:571,1,2,2-Tetrachloroethane 10.0 ug/kg 1 8260B5030ADW3.25 ND 11/12/2021 13:57Tetrachloroethene10.0 ug/kg 1 8260B5030ADW0.930 ND 11/12/2021 13:57Toluene2.00 ug/kg 1 8260B5030ADW1.00 ND 11/12/2021 13:571,2,3-Trichlorobenzene 10.0 ug/kg 1 8260B5030ADW1.23 ND 11/12/2021 13:571,2,4-Trichlorobenzene 10.0 ug/kg 1 8260B5030ADW2.82 ND 11/12/2021 13:571,1,1-Trichloroethane 10.0 ug/kg 1 8260B5030ADW2.03 ND 11/12/2021 13:571,1,2-Trichloroethane 10.0 ug/kg 1 8260B5030ADW1.74 ND 11/12/2021 13:57Trichloroethene10.0 ug/kg 1 8260B5030ADW1.15 ND 11/12/2021 13:57Trichlorofluoromethane10.0 ug/kg 1 8260B5030ADW3.15 ND 11/12/2021 13:571,2,3-Trichloropropane 10.0 ug/kg 1 8260B5030ADW1.74 ND 11/12/2021 13:571,2,4-Trimethylbenzene 10.0 ug/kg 1 8260B5030ADW3.19 ND 11/12/2021 13:571,3,5- Trimethylbenzene 10.0 ug/kg 1 8260B5030ADW1.23 ND 11/12/2021 13:57Vinyl acetate 50.0 ug/kg 1 8260B5030ADW10.8 ND 11/12/2021 13:57Vinyl chloride 30.0 ug/kg 1 8260B5030ADW2.79 ND 11/12/2021 13:57m,p-Xylenes 4.00 ug/kg 1 8260B5030ADW1.80 ND 11/12/2021 13:57o-Xylene 2.00 ug/kg 1 8260B5030ADW1.00 Amolk Brar, Lab Director The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Page 11 of 26Page 13 of 28 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 01221156.00 Luke Montague Nirvana Properties 11/17/2021 12:58San Diego CA, 92123 2111096Work Order No: ResultAnalyte PQL Analyzed MethodNotes DilutionUnits Laboratory Sample ID: 2111096-07 (Solid) Prep Method Analyst Client Sample ID: SB4-0.5 Analytical Results MDL Volatile Organic Compounds Batch ID:BK10607 Prepared:11/11/2021 17:00 11/12/2021 13:5770-12087.9 %Surrogate: 4-Bromofluorobenzene 8260B5030ADW 11/12/2021 13:5770-12074.1 %Surrogate: Dibromofluoromethane 8260B5030ADW 11/12/2021 13:5770-12092.8 %Surrogate: Toluene-d8 8260B5030ADW 8270 PAH SIM Batch ID:BK10609 Prepared:11/15/2021 09:10 ND 11/15/2021 17:11Acenaphthene20.0 ug/kg 4 8270C3550 SV AY5.52 ND 11/15/2021 17:11Acenaphthylene20.0 ug/kg 4 8270C3550 SV AY5.52 ND 11/15/2021 17:11Anthracene20.0 ug/kg 4 8270C3550 SV AY4.96 4.00 11/15/2021 17:11Benzo(a)anthracene 20.0J ug/kg 4 8270C3550 SV AY3.40 ND 11/15/2021 17:11Benzo[a]pyrene 20.0 ug/kg 4 8270C3550 SV AY9.20 ND 11/15/2021 17:11Benzo[b]fluoranthene 20.0 ug/kg 4 8270C3550 SV AY9.24 ND 11/15/2021 17:11Benzo(ghi)perylene 20.0 ug/kg 4 8270C3550 SV AY20.0 ND 11/15/2021 17:11Benzo[k]fluoranthene 20.0 ug/kg 4 8270C3550 SV AY9.72 15.3 11/15/2021 17:11Chrysene20.0J ug/kg 4 8270C3550 SV AY5.68 ND 11/15/2021 17:11Dibenz(a,h)anthracene 20.0 ug/kg 4 8270C3550 SV AY18.9 9.33 11/15/2021 17:11Fluoranthene20.0J ug/kg 4 8270C3550 SV AY4.16 ND 11/15/2021 17:11Fluorene20.0 ug/kg 4 8270C3550 SV AY5.00 ND 11/15/2021 17:11Indeno (1,2,3-cd) pyrene 20.0 ug/kg 4 8270C3550 SV AY17.7 ND 11/15/2021 17:11Naphthalene20.0 ug/kg 4 8270C3550 SV AY6.32 ND 11/15/2021 17:11Phenanthrene20.0 ug/kg 4 8270C3550 SV AY5.80 10.0 11/15/2021 17:11Pyrene20.0J ug/kg 4 8270C3550 SV AY4.12 11/15/2021 17:1135-11485.6 %Surrogate: Nitrobenzene-d5 8270C3550 SV AY 11/15/2021 17:1121-10532.4 %Surrogate: 1,4-Dioxane-d8 8270C3550 SV AY ResultAnalyte PQL Analyzed MethodNotes DilutionUnits Laboratory Sample ID: 2111096-10 (Solid) Prep Method Analyst Client Sample ID: SB5-0.5 Analytical Results MDL Total Petroleum Hydrocarbons(TPH-g)Batch ID:BK10608 Prepared:11/11/2021 17:00 ND 11/12/2021 16:45Gasoline Range Organics 500 ug/kg 1 8015B5030ADW250 11/12/2021 16:4570-120113 %Surrogate: Bromofluorobenzene 8015B5030ADW Total Petroleum Hydrocarbons(TPH DROORO)Batch ID:BK10606 Prepared:11/12/2021 10:00 ND 11/13/2021 00:50Diesel range organics 10.0 mg/kg 1 8015B3550BDW1.00 Amolk Brar, Lab Director The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Page 12 of 26Page 14 of 28 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 01221156.00 Luke Montague Nirvana Properties 11/17/2021 12:58San Diego CA, 92123 2111096Work Order No: ResultAnalyte PQL Analyzed MethodNotes DilutionUnits Laboratory Sample ID: 2111096-10 (Solid) Prep Method Analyst Client Sample ID: SB5-0.5 Analytical Results MDL Total Petroleum Hydrocarbons(TPH DROORO)Batch ID:BK10606 Prepared:11/12/2021 10:00 ND 11/13/2021 00:50Oil Range Organics 50.0 mg/kg 1 8015B3550BDW17.0 11/13/2021 00:5070-12098.2 %Surrogate: Chlorobenzene 8015B3550BDW Volatile Organic Compounds Batch ID:BK10607 Prepared:11/11/2021 17:00 ND 11/12/2021 14:23Acetone50.0 ug/kg 1 8260B5030ADW12.7 ND 11/12/2021 14:23Benzene2.00 ug/kg 1 8260B5030ADW0.930 ND 11/12/2021 14:23Bromobenzene10.0 ug/kg 1 8260B5030ADW3.39 ND 11/12/2021 14:23Bromochloromethane10.0 ug/kg 1 8260B5030ADW0.380 ND 11/12/2021 14:23Bromodichloromethane10.0 ug/kg 1 8260B5030ADW0.630 ND 11/12/2021 14:23Bromoform50.0 ug/kg 1 8260B5030ADW3.39 ND 11/12/2021 14:23Bromomethane30.0 ug/kg 1 8260B5030ADW2.75 ND 11/12/2021 14:232-Butanone 50.0 ug/kg 1 8260B5030ADW5.83 ND 11/12/2021 14:23n-Butylbenzene 10.0 ug/kg 1 8260B5030ADW2.05 ND 11/12/2021 14:23sec-Butylbenzene 10.0 ug/kg 1 8260B5030ADW3.04 ND 11/12/2021 14:23tert-Butylbenzene 10.0 ug/kg 1 8260B5030ADW1.34 ND 11/12/2021 14:23Carbon disulfide 10.0 ug/kg 1 8260B5030ADW5.53 ND 11/12/2021 14:23Carbon tetrachloride 10.0 ug/kg 1 8260B5030ADW2.48 ND 11/12/2021 14:23Chlorobenzene10.0 ug/kg 1 8260B5030ADW0.890 ND 11/12/2021 14:23Chloroethane30.0 ug/kg 1 8260B5030ADW2.15 ND 11/12/2021 14:232-Chloroethylvinyl Ether 50.0 ug/kg 1 8260B5030ADW5.53 ND 11/12/2021 14:23Chloroform10.0 ug/kg 1 8260B5030ADW1.24 ND 11/12/2021 14:23Chloromethane30.0 ug/kg 1 8260B5030ADW1.74 ND 11/12/2021 14:234-Chlorotoluene 10.0 ug/kg 1 8260B5030ADW1.34 ND 11/12/2021 14:232-Chlorotoluene 10.0 ug/kg 1 8260B5030ADW2.35 ND 11/12/2021 14:231,2-Dibromo-3-chloropropane 50.0 ug/kg 1 8260B5030ADW2.69 ND 11/12/2021 14:23Dibromochloromethane10.0 ug/kg 1 8260B5030ADW0.650 ND 11/12/2021 14:231,2-Dibromoethane 10.0 ug/kg 1 8260B5030ADW2.75 ND 11/12/2021 14:23Dibromomethane10.0 ug/kg 1 8260B5030ADW2.30 ND 11/12/2021 14:231,2-Dichlorobenzene 10.0 ug/kg 1 8260B5030ADW1.65 ND 11/12/2021 14:231,3-Dichlorobenzene 10.0 ug/kg 1 8260B5030ADW1.03 ND 11/12/2021 14:231,4-Dichlorobenzene 10.0 ug/kg 1 8260B5030ADW2.23 ND 11/12/2021 14:23Dichlorodifluoromethane30.0 ug/kg 1 8260B5030ADW2.07 ND 11/12/2021 14:231,1-Dichloroethane 10.0 ug/kg 1 8260B5030ADW1.30 ND 11/12/2021 14:231,2-Dichloroethane 10.0 ug/kg 1 8260B5030ADW1.57 ND 11/12/2021 14:231,1-Dichloroethene 10.0 ug/kg 1 8260B5030ADW1.60 ND 11/12/2021 14:23cis-1,2-Dichloroethene 10.0 ug/kg 1 8260B5030ADW2.16 Amolk Brar, Lab Director The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Page 13 of 26Page 15 of 28 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 01221156.00 Luke Montague Nirvana Properties 11/17/2021 12:58San Diego CA, 92123 2111096Work Order No: ResultAnalyte PQL Analyzed MethodNotes DilutionUnits Laboratory Sample ID: 2111096-10 (Solid) Prep Method Analyst Client Sample ID: SB5-0.5 Analytical Results MDL Volatile Organic Compounds Batch ID:BK10607 Prepared:11/11/2021 17:00 ND 11/12/2021 14:23trans-1,2-Dichloroethene 10.0 ug/kg 1 8260B5030ADW2.60 ND 11/12/2021 14:231,1-Dichloropropene 10.0 ug/kg 1 8260B5030ADW0.660 ND 11/12/2021 14:231,2-Dichloropropane 10.0 ug/kg 1 8260B5030ADW0.920 ND 11/12/2021 14:231,3-Dichloropropane 10.0 ug/kg 1 8260B5030ADW1.36 ND 11/12/2021 14:232,2-Dichloropropane 10.0 ug/kg 1 8260B5030ADW1.12 ND 11/12/2021 14:23cis-1,3-Dichloropropene 10.0 ug/kg 1 8260B5030ADW0.980 ND 11/12/2021 14:23trans-1,3-Dichloropropene 10.0 ug/kg 1 8260B5030ADW0.960 ND 11/12/2021 14:23Ethylbenzene2.00 ug/kg 1 8260B5030ADW1.00 ND 11/12/2021 14:23Hexachlorobutadiene30.0 ug/kg 1 8260B5030ADW2.77 ND 11/12/2021 14:232-Hexanone 50.0 ug/kg 1 8260B5030ADW3.18 ND 11/12/2021 14:23Isopropylbenzene10.0 ug/kg 1 8260B5030ADW1.42 ND 11/12/2021 14:23p-Isopropyltoluene 10.0 ug/kg 1 8260B5030ADW3.86 ND 11/12/2021 14:23Methyl tert-Butyl Ether (MTBE)5.00 ug/kg 1 8260B5030ADW1.81 ND 11/12/2021 14:234-Methyl-2-pentanone (MIBK)50.0 ug/kg 1 8260B5030ADW3.14 ND 11/12/2021 14:23Methylene chloride 50.0 ug/kg 1 8260B5030ADW3.31 ND 11/12/2021 14:23Naphthalene10.0 ug/kg 1 8260B5030ADW1.14 ND 11/12/2021 14:23n-Propylbenzene 10.0 ug/kg 1 8260B5030ADW1.14 ND 11/12/2021 14:23Styrene10.0 ug/kg 1 8260B5030ADW0.800 ND 11/12/2021 14:231,1,1,2-Tetrachloroethane 10.0 ug/kg 1 8260B5030ADW1.28 ND 11/12/2021 14:231,1,2,2-Tetrachloroethane 10.0 ug/kg 1 8260B5030ADW3.25 ND 11/12/2021 14:23Tetrachloroethene10.0 ug/kg 1 8260B5030ADW0.930 ND 11/12/2021 14:23Toluene2.00 ug/kg 1 8260B5030ADW1.00 ND 11/12/2021 14:231,2,3-Trichlorobenzene 10.0 ug/kg 1 8260B5030ADW1.23 ND 11/12/2021 14:231,2,4-Trichlorobenzene 10.0 ug/kg 1 8260B5030ADW2.82 ND 11/12/2021 14:231,1,1-Trichloroethane 10.0 ug/kg 1 8260B5030ADW2.03 ND 11/12/2021 14:231,1,2-Trichloroethane 10.0 ug/kg 1 8260B5030ADW1.74 ND 11/12/2021 14:23Trichloroethene10.0 ug/kg 1 8260B5030ADW1.15 ND 11/12/2021 14:23Trichlorofluoromethane10.0 ug/kg 1 8260B5030ADW3.15 ND 11/12/2021 14:231,2,3-Trichloropropane 10.0 ug/kg 1 8260B5030ADW1.74 ND 11/12/2021 14:231,2,4-Trimethylbenzene 10.0 ug/kg 1 8260B5030ADW3.19 ND 11/12/2021 14:231,3,5- Trimethylbenzene 10.0 ug/kg 1 8260B5030ADW1.23 ND 11/12/2021 14:23Vinyl acetate 50.0 ug/kg 1 8260B5030ADW10.8 ND 11/12/2021 14:23Vinyl chloride 30.0 ug/kg 1 8260B5030ADW2.79 ND 11/12/2021 14:23m,p-Xylenes 4.00 ug/kg 1 8260B5030ADW1.80 ND 11/12/2021 14:23o-Xylene 2.00 ug/kg 1 8260B5030ADW1.00 11/12/2021 14:2370-12086.1 %Surrogate: 4-Bromofluorobenzene 8260B5030ADW Amolk Brar, Lab Director The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Page 14 of 26Page 16 of 28 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 01221156.00 Luke Montague Nirvana Properties 11/17/2021 12:58San Diego CA, 92123 2111096Work Order No: ResultAnalyte PQL Analyzed MethodNotes DilutionUnits Laboratory Sample ID: 2111096-10 (Solid) Prep Method Analyst Client Sample ID: SB5-0.5 Analytical Results MDL Volatile Organic Compounds Batch ID:BK10607 Prepared:11/11/2021 17:00 11/12/2021 14:2370-12072.0 %Surrogate: Dibromofluoromethane 8260B5030ADW 11/12/2021 14:2370-12093.9 %Surrogate: Toluene-d8 8260B5030ADW 8270 PAH SIM Batch ID:BK10609 Prepared:11/15/2021 09:10 ND 11/15/2021 17:42Acenaphthene5.00 ug/kg 1 8270C3550 SV AY1.38 ND 11/15/2021 17:42Acenaphthylene5.00 ug/kg 1 8270C3550 SV AY1.38 ND 11/15/2021 17:42Anthracene5.00 ug/kg 1 8270C3550 SV AY1.24 ND 11/15/2021 17:42Benzo(a)anthracene 5.00 ug/kg 1 8270C3550 SV AY0.849 ND 11/15/2021 17:42Benzo[a]pyrene 5.00 ug/kg 1 8270C3550 SV AY2.30 ND 11/15/2021 17:42Benzo[b]fluoranthene 5.00 ug/kg 1 8270C3550 SV AY2.31 ND 11/15/2021 17:42Benzo(ghi)perylene 5.00 ug/kg 1 8270C3550 SV AY5.00 ND 11/15/2021 17:42Benzo[k]fluoranthene 5.00 ug/kg 1 8270C3550 SV AY2.43 ND 11/15/2021 17:42Chrysene5.00 ug/kg 1 8270C3550 SV AY1.42 ND 11/15/2021 17:42Dibenz(a,h)anthracene 5.00 ug/kg 1 8270C3550 SV AY4.73 ND 11/15/2021 17:42Fluoranthene5.00 ug/kg 1 8270C3550 SV AY1.04 ND 11/15/2021 17:42Fluorene5.00 ug/kg 1 8270C3550 SV AY1.25 ND 11/15/2021 17:42Indeno (1,2,3-cd) pyrene 5.00 ug/kg 1 8270C3550 SV AY4.42 ND 11/15/2021 17:42Naphthalene5.00 ug/kg 1 8270C3550 SV AY1.58 ND 11/15/2021 17:42Phenanthrene5.00 ug/kg 1 8270C3550 SV AY1.45 ND 11/15/2021 17:42Pyrene5.00 ug/kg 1 8270C3550 SV AY1.03 11/15/2021 17:4235-11478.1 %Surrogate: Nitrobenzene-d5 8270C3550 SV AY 11/15/2021 17:4221-10533.2 %Surrogate: 1,4-Dioxane-d8 8270C3550 SV AY ResultAnalyte PQL Analyzed MethodNotes DilutionUnits Laboratory Sample ID: 2111096-13 (Solid) Prep Method Analyst Client Sample ID: SB6-0.5 Analytical Results MDL Total Petroleum Hydrocarbons(TPH-g)Batch ID:BK10608 Prepared:11/11/2021 17:00 ND 11/12/2021 17:14Gasoline Range Organics 500 ug/kg 1 8015B5030ADW250 11/12/2021 17:1470-120100 %Surrogate: Bromofluorobenzene 8015B5030ADW Total Petroleum Hydrocarbons(TPH DROORO)Batch ID:BK10606 Prepared:11/12/2021 10:00 ND 11/13/2021 01:32Diesel range organics 10.0 mg/kg 1 8015B3550BDW1.00 ND 11/13/2021 01:32Oil Range Organics 50.0 mg/kg 1 8015B3550BDW17.0 Amolk Brar, Lab Director The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Page 15 of 26Page 17 of 28 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 01221156.00 Luke Montague Nirvana Properties 11/17/2021 12:58San Diego CA, 92123 2111096Work Order No: ResultAnalyte PQL Analyzed MethodNotes DilutionUnits Laboratory Sample ID: 2111096-13 (Solid) Prep Method Analyst Client Sample ID: SB6-0.5 Analytical Results MDL Total Petroleum Hydrocarbons(TPH DROORO)Batch ID:BK10606 Prepared:11/12/2021 10:00 11/13/2021 01:3270-12099.9 %Surrogate: Chlorobenzene 8015B3550BDW Volatile Organic Compounds Batch ID:BK10607 Prepared:11/11/2021 17:00 ND 11/12/2021 15:14Acetone50.0 ug/kg 1 8260B5030ADW12.7 ND 11/12/2021 15:14Benzene2.00 ug/kg 1 8260B5030ADW0.930 ND 11/12/2021 15:14Bromobenzene10.0 ug/kg 1 8260B5030ADW3.39 ND 11/12/2021 15:14Bromochloromethane10.0 ug/kg 1 8260B5030ADW0.380 ND 11/12/2021 15:14Bromodichloromethane10.0 ug/kg 1 8260B5030ADW0.630 ND 11/12/2021 15:14Bromoform50.0 ug/kg 1 8260B5030ADW3.39 ND 11/12/2021 15:14Bromomethane30.0 ug/kg 1 8260B5030ADW2.75 ND 11/12/2021 15:142-Butanone 50.0 ug/kg 1 8260B5030ADW5.83 ND 11/12/2021 15:14n-Butylbenzene 10.0 ug/kg 1 8260B5030ADW2.05 ND 11/12/2021 15:14sec-Butylbenzene 10.0 ug/kg 1 8260B5030ADW3.04 ND 11/12/2021 15:14tert-Butylbenzene 10.0 ug/kg 1 8260B5030ADW1.34 ND 11/12/2021 15:14Carbon disulfide 10.0 ug/kg 1 8260B5030ADW5.53 ND 11/12/2021 15:14Carbon tetrachloride 10.0 ug/kg 1 8260B5030ADW2.48 ND 11/12/2021 15:14Chlorobenzene10.0 ug/kg 1 8260B5030ADW0.890 ND 11/12/2021 15:14Chloroethane30.0 ug/kg 1 8260B5030ADW2.15 ND 11/12/2021 15:142-Chloroethylvinyl Ether 50.0 ug/kg 1 8260B5030ADW5.53 ND 11/12/2021 15:14Chloroform10.0 ug/kg 1 8260B5030ADW1.24 ND 11/12/2021 15:14Chloromethane30.0 ug/kg 1 8260B5030ADW1.74 ND 11/12/2021 15:144-Chlorotoluene 10.0 ug/kg 1 8260B5030ADW1.34 ND 11/12/2021 15:142-Chlorotoluene 10.0 ug/kg 1 8260B5030ADW2.35 ND 11/12/2021 15:141,2-Dibromo-3-chloropropane 50.0 ug/kg 1 8260B5030ADW2.69 ND 11/12/2021 15:14Dibromochloromethane10.0 ug/kg 1 8260B5030ADW0.650 ND 11/12/2021 15:141,2-Dibromoethane 10.0 ug/kg 1 8260B5030ADW2.75 ND 11/12/2021 15:14Dibromomethane10.0 ug/kg 1 8260B5030ADW2.30 ND 11/12/2021 15:141,2-Dichlorobenzene 10.0 ug/kg 1 8260B5030ADW1.65 ND 11/12/2021 15:141,3-Dichlorobenzene 10.0 ug/kg 1 8260B5030ADW1.03 ND 11/12/2021 15:141,4-Dichlorobenzene 10.0 ug/kg 1 8260B5030ADW2.23 ND 11/12/2021 15:14Dichlorodifluoromethane30.0 ug/kg 1 8260B5030ADW2.07 ND 11/12/2021 15:141,1-Dichloroethane 10.0 ug/kg 1 8260B5030ADW1.30 ND 11/12/2021 15:141,2-Dichloroethane 10.0 ug/kg 1 8260B5030ADW1.57 ND 11/12/2021 15:141,1-Dichloroethene 10.0 ug/kg 1 8260B5030ADW1.60 ND 11/12/2021 15:14cis-1,2-Dichloroethene 10.0 ug/kg 1 8260B5030ADW2.16 ND 11/12/2021 15:14trans-1,2-Dichloroethene 10.0 ug/kg 1 8260B5030ADW2.60 Amolk Brar, Lab Director The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Page 16 of 26Page 18 of 28 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 01221156.00 Luke Montague Nirvana Properties 11/17/2021 12:58San Diego CA, 92123 2111096Work Order No: ResultAnalyte PQL Analyzed MethodNotes DilutionUnits Laboratory Sample ID: 2111096-13 (Solid) Prep Method Analyst Client Sample ID: SB6-0.5 Analytical Results MDL Volatile Organic Compounds Batch ID:BK10607 Prepared:11/11/2021 17:00 ND 11/12/2021 15:141,1-Dichloropropene 10.0 ug/kg 1 8260B5030ADW0.660 ND 11/12/2021 15:141,2-Dichloropropane 10.0 ug/kg 1 8260B5030ADW0.920 ND 11/12/2021 15:141,3-Dichloropropane 10.0 ug/kg 1 8260B5030ADW1.36 ND 11/12/2021 15:142,2-Dichloropropane 10.0 ug/kg 1 8260B5030ADW1.12 ND 11/12/2021 15:14cis-1,3-Dichloropropene 10.0 ug/kg 1 8260B5030ADW0.980 ND 11/12/2021 15:14trans-1,3-Dichloropropene 10.0 ug/kg 1 8260B5030ADW0.960 ND 11/12/2021 15:14Ethylbenzene2.00 ug/kg 1 8260B5030ADW1.00 ND 11/12/2021 15:14Hexachlorobutadiene30.0 ug/kg 1 8260B5030ADW2.77 ND 11/12/2021 15:142-Hexanone 50.0 ug/kg 1 8260B5030ADW3.18 ND 11/12/2021 15:14Isopropylbenzene10.0 ug/kg 1 8260B5030ADW1.42 ND 11/12/2021 15:14p-Isopropyltoluene 10.0 ug/kg 1 8260B5030ADW3.86 ND 11/12/2021 15:14Methyl tert-Butyl Ether (MTBE)5.00 ug/kg 1 8260B5030ADW1.81 ND 11/12/2021 15:144-Methyl-2-pentanone (MIBK)50.0 ug/kg 1 8260B5030ADW3.14 ND 11/12/2021 15:14Methylene chloride 50.0 ug/kg 1 8260B5030ADW3.31 ND 11/12/2021 15:14Naphthalene10.0 ug/kg 1 8260B5030ADW1.14 ND 11/12/2021 15:14n-Propylbenzene 10.0 ug/kg 1 8260B5030ADW1.14 ND 11/12/2021 15:14Styrene10.0 ug/kg 1 8260B5030ADW0.800 ND 11/12/2021 15:141,1,1,2-Tetrachloroethane 10.0 ug/kg 1 8260B5030ADW1.28 ND 11/12/2021 15:141,1,2,2-Tetrachloroethane 10.0 ug/kg 1 8260B5030ADW3.25 ND 11/12/2021 15:14Tetrachloroethene10.0 ug/kg 1 8260B5030ADW0.930 ND 11/12/2021 15:14Toluene2.00 ug/kg 1 8260B5030ADW1.00 ND 11/12/2021 15:141,2,3-Trichlorobenzene 10.0 ug/kg 1 8260B5030ADW1.23 ND 11/12/2021 15:141,2,4-Trichlorobenzene 10.0 ug/kg 1 8260B5030ADW2.82 ND 11/12/2021 15:141,1,1-Trichloroethane 10.0 ug/kg 1 8260B5030ADW2.03 ND 11/12/2021 15:141,1,2-Trichloroethane 10.0 ug/kg 1 8260B5030ADW1.74 ND 11/12/2021 15:14Trichloroethene10.0 ug/kg 1 8260B5030ADW1.15 ND 11/12/2021 15:14Trichlorofluoromethane10.0 ug/kg 1 8260B5030ADW3.15 ND 11/12/2021 15:141,2,3-Trichloropropane 10.0 ug/kg 1 8260B5030ADW1.74 ND 11/12/2021 15:141,2,4-Trimethylbenzene 10.0 ug/kg 1 8260B5030ADW3.19 ND 11/12/2021 15:141,3,5- Trimethylbenzene 10.0 ug/kg 1 8260B5030ADW1.23 ND 11/12/2021 15:14Vinyl acetate 50.0 ug/kg 1 8260B5030ADW10.8 ND 11/12/2021 15:14Vinyl chloride 30.0 ug/kg 1 8260B5030ADW2.79 ND 11/12/2021 15:14m,p-Xylenes 4.00 ug/kg 1 8260B5030ADW1.80 ND 11/12/2021 15:14o-Xylene 2.00 ug/kg 1 8260B5030ADW1.00 11/12/2021 15:1470-12087.4 %Surrogate: 4-Bromofluorobenzene 8260B5030ADW 11/12/2021 15:1470-12073.7 %Surrogate: Dibromofluoromethane 8260B5030ADW Amolk Brar, Lab Director The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Page 17 of 26Page 19 of 28 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 01221156.00 Luke Montague Nirvana Properties 11/17/2021 12:58San Diego CA, 92123 2111096Work Order No: ResultAnalyte PQL Analyzed MethodNotes DilutionUnits Laboratory Sample ID: 2111096-13 (Solid) Prep Method Analyst Client Sample ID: SB6-0.5 Analytical Results MDL Volatile Organic Compounds Batch ID:BK10607 Prepared:11/11/2021 17:00 11/12/2021 15:1470-12091.9 %Surrogate: Toluene-d8 8260B5030ADW 8270 PAH SIM Batch ID:BK10609 Prepared:11/15/2021 09:10 ND 11/15/2021 18:12Acenaphthene5.00 ug/kg 1 8270C3550 SV AY1.38 ND 11/15/2021 18:12Acenaphthylene5.00 ug/kg 1 8270C3550 SV AY1.38 ND 11/15/2021 18:12Anthracene5.00 ug/kg 1 8270C3550 SV AY1.24 ND 11/15/2021 18:12Benzo(a)anthracene 5.00 ug/kg 1 8270C3550 SV AY0.849 ND 11/15/2021 18:12Benzo[a]pyrene 5.00 ug/kg 1 8270C3550 SV AY2.30 ND 11/15/2021 18:12Benzo[b]fluoranthene 5.00 ug/kg 1 8270C3550 SV AY2.31 ND 11/15/2021 18:12Benzo(ghi)perylene 5.00 ug/kg 1 8270C3550 SV AY5.00 ND 11/15/2021 18:12Benzo[k]fluoranthene 5.00 ug/kg 1 8270C3550 SV AY2.43 ND 11/15/2021 18:12Chrysene5.00 ug/kg 1 8270C3550 SV AY1.42 ND 11/15/2021 18:12Dibenz(a,h)anthracene 5.00 ug/kg 1 8270C3550 SV AY4.73 ND 11/15/2021 18:12Fluoranthene5.00 ug/kg 1 8270C3550 SV AY1.04 ND 11/15/2021 18:12Fluorene5.00 ug/kg 1 8270C3550 SV AY1.25 ND 11/15/2021 18:12Indeno (1,2,3-cd) pyrene 5.00 ug/kg 1 8270C3550 SV AY4.42 ND 11/15/2021 18:12Naphthalene5.00 ug/kg 1 8270C3550 SV AY1.58 ND 11/15/2021 18:12Phenanthrene5.00 ug/kg 1 8270C3550 SV AY1.45 ND 11/15/2021 18:12Pyrene5.00 ug/kg 1 8270C3550 SV AY1.03 11/15/2021 18:1235-11489.7 %Surrogate: Nitrobenzene-d5 8270C3550 SV AY 11/15/2021 18:1221-10536.6 %Surrogate: 1,4-Dioxane-d8 8270C3550 SV AY Amolk Brar, Lab Director The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Page 18 of 26Page 20 of 28 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 01221156.00 Luke Montague Nirvana Properties 11/17/2021 12:58San Diego CA, 92123 2111096Work Order No: Result Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Total Petroleum Hydrocarbons(TPH-g) - Quality Control Report PQLMDL Batch BK10608 - 5030A - 8015B Blank (BK10608-BLK1)Prepared: 11/11/202 Analyzed: 11/12/202 Gasoline Range Organics ug/kgND500250 LCS (BK10608-BS1)Prepared: 11/11/202 Analyzed: 11/12/202 Gasoline Range Organics ug/L563 500 75-120113 LCS Dup (BK10608-BSD1)Prepared: 11/11/202 Analyzed: 11/12/202 Gasoline Range Organics ug/L562 500 1575-120112 0.105 Matrix Spike (BK10608-MS1)Prepared: 11/11/202 Analyzed: 11/12/202Source: 2111096-10 Gasoline Range Organics ug/L550 500 0.00 75-120110 Matrix Spike Dup (BK10608-MSD1)Prepared: 11/11/202 Analyzed: 11/12/202Source: 2111096-10 Gasoline Range Organics ug/L557 500 0.00 1575-120111 1.30 Amolk Brar, Lab Director The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Page 19 of 26Page 21 of 28 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 01221156.00 Luke Montague Nirvana Properties 11/17/2021 12:58San Diego CA, 92123 2111096Work Order No: Result Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Total Petroleum Hydrocarbons(TPH DROORO) - Quality Control Report PQLMDL Batch BK10606 - 3550B - 8015B Blank (BK10606-BLK1)Prepared: 11/12/202 Analyzed: 11/13/202 Diesel range organics mg/kgND10.01.00 Oil Range Organics "ND 50.017.0 mg/L 100 70-120Surrogate: Chlorobenzene 92.992.9 LCS (BK10606-BS1)Prepared: 11/12/202 Analyzed: 11/13/202 Diesel range organics mg/L551 500 75-120110 "100 70-120Surrogate: Chlorobenzene 106106 LCS Dup (BK10606-BSD1)Prepared: 11/12/202 Analyzed: 11/13/202 Diesel range organics mg/L558 500 2075-120112 1.20 "100 70-120Surrogate: Chlorobenzene 105105 Matrix Spike (BK10606-MS1)Prepared: 11/12/202 Analyzed: 11/13/202Source: 2111096-10 Diesel range organics mg/L547 500 0.00 75-120109 "100 70-120Surrogate: Chlorobenzene 104104 Matrix Spike Dup (BK10606-MSD1)Prepared: 11/12/202 Analyzed: 11/13/202Source: 2111096-10 Diesel range organics mg/L550 500 0.00 2075-120110 0.622 "100 70-120Surrogate: Chlorobenzene 105105 Amolk Brar, Lab Director The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Page 20 of 26Page 22 of 28 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 01221156.00 Luke Montague Nirvana Properties 11/17/2021 12:58San Diego CA, 92123 2111096Work Order No: Result Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds - Quality Control Report PQLMDL Batch BK10607 - 5030A - 8260B Blank (BK10607-BLK1)Prepared: 11/11/202 Analyzed: 11/12/202 Acetone ug/kgND50.012.7 Benzene "ND 2.000.930 Bromobenzene "ND 10.03.39 Bromochloromethane "ND 10.00.380 Bromodichloromethane "ND 10.00.630 Bromoform "ND 50.03.39 Bromomethane "ND 30.02.75 2-Butanone "ND 50.05.83 n-Butylbenzene "ND 10.02.05 sec-Butylbenzene "ND 10.03.04 tert-Butylbenzene "ND 10.01.34 Carbon disulfide "ND 10.05.53 Carbon tetrachloride "ND 10.02.48 Chlorobenzene "ND 10.00.890 Chloroethane "ND 30.02.15 2-Chloroethylvinyl Ether "ND 50.05.53 Chloroform "ND 10.01.24 Chloromethane "ND 30.01.74 4-Chlorotoluene "ND 10.01.34 2-Chlorotoluene "ND 10.02.35 1,2-Dibromo-3-chloropropane "ND 50.02.69 Dibromochloromethane "ND 10.00.650 1,2-Dibromoethane "ND 10.02.75 Dibromomethane "ND 10.02.30 1,2-Dichlorobenzene "ND 10.01.65 1,3-Dichlorobenzene "ND 10.01.03 1,4-Dichlorobenzene "ND 10.02.23 Dichlorodifluoromethane "ND 30.02.07 1,1-Dichloroethane "ND 10.01.30 1,2-Dichloroethane "ND 10.01.57 1,1-Dichloroethene "ND 10.01.60 cis-1,2-Dichloroethene "ND 10.02.16 trans-1,2-Dichloroethene "ND 10.02.60 1,1-Dichloropropene "ND 10.00.660 1,2-Dichloropropane "ND 10.00.920 1,3-Dichloropropane "ND 10.01.36 2,2-Dichloropropane "ND 10.01.12 cis-1,3-Dichloropropene "ND 10.00.980 trans-1,3-Dichloropropene "ND 10.00.960 Ethylbenzene "ND 2.001.00 Hexachlorobutadiene "ND 30.02.77 Amolk Brar, Lab Director The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Page 21 of 26Page 23 of 28 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 01221156.00 Luke Montague Nirvana Properties 11/17/2021 12:58San Diego CA, 92123 2111096Work Order No: Result Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds - Quality Control Report PQLMDL Batch BK10607 - 5030A - 8260B Blank (BK10607-BLK1)Prepared: 11/11/202 Analyzed: 11/12/202 2-Hexanone ug/kgND50.03.18 Isopropylbenzene "ND 10.01.42 p-Isopropyltoluene "ND 10.03.86 Methyl tert-Butyl Ether (MTBE)"ND 5.001.81 4-Methyl-2-pentanone (MIBK)"ND 50.03.14 Methylene chloride "ND 50.03.31 Naphthalene "ND 10.01.14 n-Propylbenzene "ND 10.01.14 Styrene "ND 10.00.800 1,1,1,2-Tetrachloroethane "ND 10.01.28 1,1,2,2-Tetrachloroethane "ND 10.03.25 Tetrachloroethene "ND 10.00.930 Toluene "ND 2.001.00 1,2,3-Trichlorobenzene "ND 10.01.23 1,2,4-Trichlorobenzene "ND 10.02.82 1,1,1-Trichloroethane "ND 10.02.03 1,1,2-Trichloroethane "ND 10.01.74 Trichloroethene "ND 10.01.15 Trichlorofluoromethane "ND 10.03.15 1,2,3-Trichloropropane "ND 10.01.74 1,2,4-Trimethylbenzene "ND 10.03.19 1,3,5- Trimethylbenzene "ND 10.01.23 Vinyl acetate "ND 50.010.8 Vinyl chloride "ND 30.02.79 m,p-Xylenes "ND 4.001.80 o-Xylene "ND 2.001.00 LCS (BK10607-BS1)Prepared: 11/11/202 Analyzed: 11/12/202 Benzene ug/L53.4 50.0 75-120107 Chlorobenzene "50.2 50.0 75-120100 1,1-Dichloroethene "55.5 50.0 75-120111 Methyl tert-Butyl Ether (MTBE)"44.4 50.0 75-12088.8 Toluene "44.7 50.0 75-12089.5 Trichloroethene "43.8 50.0 75-12087.6 Amolk Brar, Lab Director The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Page 22 of 26Page 24 of 28 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 01221156.00 Luke Montague Nirvana Properties 11/17/2021 12:58San Diego CA, 92123 2111096Work Order No: Result Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds - Quality Control Report PQLMDL Batch BK10607 - 5030A - 8260B LCS Dup (BK10607-BSD1)Prepared: 11/11/202 Analyzed: 11/12/202 Benzene ug/L55.4 50.0 2075-120111 3.77 Chlorobenzene "50.4 50.0 2075-120101 0.438 1,1-Dichloroethene "60.1 50.0 1575-120120 7.87 Methyl tert-Butyl Ether (MTBE)"45.5 50.0 1575-12091.0 2.47 Toluene "43.1 50.0 1575-12086.2 3.73 Trichloroethene "45.0 50.0 2075-12089.9 2.64 Matrix Spike (BK10607-MS1)Prepared: 11/11/202 Analyzed: 11/12/202Source: 2111096-10 Benzene ug/L49.4 50.0 0.00 75-12098.9 Chlorobenzene "47.8 50.0 0.00 75-12095.5 1,1-Dichloroethene "51.7 50.0 0.00 75-120103 Methyl tert-Butyl Ether (MTBE)"38.5 50.0 0.00 75-12077.0 Toluene "40.7 50.0 0.00 75-12081.4 Trichloroethene "40.6 50.0 0.00 75-12081.1 Matrix Spike Dup (BK10607-MSD1)Prepared: 11/11/202 Analyzed: 11/12/202Source: 2111096-10 Benzene ug/L53.4 50.0 0.00 1575-120107 7.80 Chlorobenzene "49.6 50.0 0.00 1575-12099.1 3.72 1,1-Dichloroethene "56.1 50.0 0.00 1575-120112 8.09 Methyl tert-Butyl Ether (MTBE)"43.8 50.0 0.00 1575-12087.7 12.9 Toluene "43.5 50.0 0.00 1575-12087.0 6.65 Trichloroethene "43.9 50.0 0.00 1575-12087.7 7.84 Amolk Brar, Lab Director The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Page 23 of 26Page 25 of 28 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 01221156.00 Luke Montague Nirvana Properties 11/17/2021 12:58San Diego CA, 92123 2111096Work Order No: Result Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte 8270 PAH SIM - Quality Control Report PQLMDL Batch BK10609 - 3550 SV - 8270C Blank (BK10609-BLK1)Prepared & Analyzed: 11/15/202 Acenaphthene ug/kgND5.001.38 Acenaphthylene "ND 5.001.38 Anthracene "ND 5.001.24 Benzo(a)anthracene "ND 5.000.849 Benzo[a]pyrene "ND 5.002.30 Benzo[b]fluoranthene "ND 5.002.31 Benzo(ghi)perylene "ND 5.005.00 Benzo[k]fluoranthene "ND 5.002.43 Chrysene "ND 5.001.42 Dibenz(a,h)anthracene "ND 5.004.73 Fluoranthene "ND 5.001.04 Fluorene "ND 5.001.25 Indeno (1,2,3-cd) pyrene "ND 5.004.42 Naphthalene "ND 5.001.58 Phenanthrene "ND 5.001.45 Pyrene "ND 5.001.03 LCS (BK10609-BS1)Prepared & Analyzed: 11/15/202 Acenaphthene ug/kg19.5 5.00 33.3 43-11858.51.38 Pyrene "18.3 5.00 33.3 26-12755.01.03 LCS Dup (BK10609-BSD1)Prepared & Analyzed: 11/15/202 Acenaphthene ug/kg19.0 5.00 33.3 3043-11857.0 2.601.38 Pyrene "18.7 5.00 33.3 3026-12756.0 1.801.03 Matrix Spike (BK10609-MS1)Prepared & Analyzed: 11/15/202Source: 2111096-13 Acenaphthene ug/kg24.5 5.00 33.3 ND 43-11873.51.38 Pyrene "26.3 5.00 33.3 ND 26-12779.01.03 Amolk Brar, Lab Director The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Page 24 of 26Page 26 of 28 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 01221156.00 Luke Montague Nirvana Properties 11/17/2021 12:58San Diego CA, 92123 2111096Work Order No: Result Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte 8270 PAH SIM - Quality Control Report PQLMDL Batch BK10609 - 3550 SV - 8270C Matrix Spike Dup (BK10609-MSD1)Prepared & Analyzed: 11/15/202Source: 2111096-13 Acenaphthene ug/kg21.8 5.00 33.3 ND 3043-11865.5 11.51.38 Pyrene "24.0 5.00 33.3 ND 3026-12772.0 9.271.03 Amolk Brar, Lab Director The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Page 25 of 26Page 27 of 28 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 01221156.00 Luke Montague Nirvana Properties 11/17/2021 12:58San Diego CA, 92123 2111096Work Order No: Notes and Definitions J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag). Sample results reported on a dry weight basis Relative Percent DifferenceRPD dry Not ReportedNR Analyte NOT DETECTED at or above the practical quantitation limit (PQL)ND Analyte DETECTEDDET Page 28 of 28 SCS Engineers - San Diego San Diego, CA 92123 8799 Balboa Avenue, Suite 290 Luke Montague Enclosed is the analytical report for the above referenced project. The data herein applies to samples as received by H&P Mobile Geochemistry, Inc. on 11-Nov-21 which were analyzed in accordance with the attached Chain of Custody record(s). The results for all sample analyses and required QA/QC analyses are presented in the following sections and summarized in the documents: •Sample Summary •Case Narrative (if applicable) •Sample Results •Quality Control Summary •Notes and Definitions / Appendix •Chain of Custody •Sampling Logs (if applicable) Unless otherwise noted, I certify that all analyses were performed and reviewed in compliance with our Quality Systems Manual and Standard Operating Procedures. This report shall not be reproduced, except in full, without the written approval of H &P Mobile Geochemistry, Inc. We at H&P Mobile Geochemistry, Inc. sincerely appreciate the opportunity to provide analytical services to you on this project. If you have any questions or concerns regarding this analytical report, please contact me at your convenience at 760-804-9678. Sincerely, 16 November 2021 Lisa Eminhizer Laboratory Director H&P Mobile Geochemistry, Inc. is certified under the California ELAP and the National Environmental Laboratory Accreditation Conference (NELAC) for the fields of proficiency and analytes listed on those certificates. H&P is approved as an Environmental Testing Laboratory in accordance with the DoD-ELAP Program and ISO/IEC 17025:2005 programs for the fields of proficiency and analytes included in the certification process and to the extent offered by the accreditation agency . Unless otherwise noted, accreditation certificate numbers, expiration of certificates, and scope of accreditation can be found at: www.handpmg.com/about/certifications . Fields of services and analytes contained in this report that are not listed on the certificates should be considered uncertified or unavailable for certification. Client Project: 01221156.00/ 821 Main Street H&P Project: SCS111221-11 Dear Luke Montague: P 1.800.834.9888 / 760.804.9678 F 760.804.9159 W handpmg.com 2470 Impala Drive, Carlsbad, CA 92010 & Field Office - Signal Hill, CAQuality. Accuracy. Experience. Geochemistry Inc. Mobile Page 1 of 13 Project: Project Number: Project Manager: Reported: SCS Engineers - San Diego 8799 Balboa Avenue, Suite 290 SCS111221-11 01221156.00/ 821 Main Street Luke MontagueSan Diego, CA 92123 16-Nov-21 15:37 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax H&P Mobile Geochemistry Inc. Sample ID Laboratory ID Matrix Date Sampled ANALYTICAL REPORT FOR SAMPLES Date Received SV3-3 E111044-01 Vapor 11-Nov-21 11-Nov-21 SV3-3 Rep E111044-02 Vapor 11-Nov-21 11-Nov-21 SV2-2 E111044-03 Vapor 11-Nov-21 11-Nov-21 SV1-4 E111044-04 Vapor 11-Nov-21 11-Nov-21 The percent recoveries for 2-Butanone, 2 Hexanone and 1,2,4-Trichlorobenzene fell below the method criteria in the continuing calibration verification. Any results for these analytes may be biased low. Page 2 of 13 Project: Project Number: Project Manager: Reported: SCS Engineers - San Diego 8799 Balboa Avenue, Suite 290 SCS111221-11 01221156.00/ 821 Main Street Luke MontagueSan Diego, CA 92123 16-Nov-21 15:37 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax H&P Mobile Geochemistry Inc. DETECTIONS SUMMARY Sample ID:Laboratory ID: Analyte Result Limit Units Method E111044-01SV3-3 Notes Reporting Toluene 9.8 3.8 ug/m3 EPA TO-15 m,p-Xylene 9.2 8.8 ug/m3 EPA TO-15 Sample ID:Laboratory ID: Analyte Result Limit Units Method E111044-02SV3-3 Rep Notes Reporting Toluene 8.8 3.8 ug/m3 EPA TO-15 Sample ID:Laboratory ID: Analyte Result Limit Units Method E111044-03SV2-2 Notes Reporting Carbon disulfide 47 6.3 ug/m3 EPA TO-15 Toluene 19 3.8 ug/m3 EPA TO-15 m,p-Xylene 26 8.8 ug/m3 EPA TO-15 o-Xylene 7.2 4.4 ug/m3 EPA TO-15 1,2,4-Trimethylbenzene 12 5.0 ug/m3 EPA TO-15 Sample ID:Laboratory ID: Analyte Result Limit Units Method E111044-04SV1-4 Notes Reporting Chloroform 9.0 4.9 ug/m3 EPA TO-15 Page 3 of 13 Project: Project Number: Project Manager: Reported: SCS Engineers - San Diego 8799 Balboa Avenue, Suite 290 SCS111221-11 01221156.00/ 821 Main Street Luke MontagueSan Diego, CA 92123 16-Nov-21 15:37 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax H&P Mobile Geochemistry Inc. Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes Factor SV3-3 (E111044-01) Vapor Sampled: 11-Nov-21 Received: 11-Nov-21 EPA TO-1515-Nov-21 15-Nov-21ug/m3 EK1150811,1-Difluoroethane (LCC)5.5ND """"""Dichlorodifluoromethane (F12)5.0ND """"""Chloromethane 2.1ND """"""Dichlorotetrafluoroethane (F114)7.1ND """"""Vinyl chloride 2.6ND """"""Bromomethane 16ND """"""Chloroethane 8.0ND """"""Trichlorofluoromethane (F11)5.6ND """"""1,1-Dichloroethene 4.0ND """"""1,1,2-Trichlorotrifluoroethane (F113)7.7ND """"""Methylene chloride (Dichloromethane)3.5ND """"""Carbon disulfide 6.3ND """"""trans-1,2-Dichloroethene 8.0ND """"""1,1-Dichloroethane 4.1ND """"""2-Butanone (MEK)30ND """"""cis-1,2-Dichloroethene 4.0ND """"""Chloroform 4.9ND """"""1,1,1-Trichloroethane 5.5ND """"""1,2-Dichloroethane (EDC)4.1ND """"""Benzene 3.2ND """"""Carbon tetrachloride 6.4ND """"""Trichloroethene 5.5ND """"""1,2-Dichloropropane 9.4ND """"""Bromodichloromethane 6.8ND """"""cis-1,3-Dichloropropene 4.6ND """"""4-Methyl-2-pentanone (MIBK)8.3ND """"""trans-1,3-Dichloropropene 4.6ND """""Toluene "3.89.8 """"""1,1,2-Trichloroethane 5.5ND """"""2-Hexanone (MBK)8.3ND """"""Dibromochloromethane 8.6ND """"""Tetrachloroethene 6.9ND """"""1,2-Dibromoethane (EDB)7.8ND """"""1,1,1,2-Tetrachloroethane 7.0ND """"""Chlorobenzene 4.7ND """"""Ethylbenzene 4.4ND """""m,p-Xylene "8.89.2 """"""Styrene 4.3ND Page 4 of 13 Project: Project Number: Project Manager: Reported: SCS Engineers - San Diego 8799 Balboa Avenue, Suite 290 SCS111221-11 01221156.00/ 821 Main Street Luke MontagueSan Diego, CA 92123 16-Nov-21 15:37 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax H&P Mobile Geochemistry Inc. Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes Factor SV3-3 (E111044-01) Vapor Sampled: 11-Nov-21 Received: 11-Nov-21 EPA TO-1515-Nov-21 15-Nov-21ug/m3 EK115081o-Xylene 4.4ND """"""Bromoform 10ND """"""1,1,2,2-Tetrachloroethane 7.0ND """"""4-Ethyltoluene 5.0ND """"""1,3,5-Trimethylbenzene 5.0ND """"""1,2,4-Trimethylbenzene 5.0ND """"""1,3-Dichlorobenzene 12ND """"""1,4-Dichlorobenzene 12ND """"""1,2-Dichlorobenzene 12ND """"""1,2,4-Trichlorobenzene 38ND """"""Hexachlorobutadiene 54ND """"107 %76-134Surrogate: 1,2-Dichloroethane-d4 """"102 %78-125Surrogate: Toluene-d8 """"85.8 %77-127Surrogate: 4-Bromofluorobenzene SV3-3 Rep (E111044-02) Vapor Sampled: 11-Nov-21 Received: 11-Nov-21 EPA TO-1515-Nov-21 15-Nov-21ug/m3 EK1150811,1-Difluoroethane (LCC)5.5ND """"""Dichlorodifluoromethane (F12)5.0ND """"""Chloromethane 2.1ND """"""Dichlorotetrafluoroethane (F114)7.1ND """"""Vinyl chloride 2.6ND """"""Bromomethane 16ND """"""Chloroethane 8.0ND """"""Trichlorofluoromethane (F11)5.6ND """"""1,1-Dichloroethene 4.0ND """"""1,1,2-Trichlorotrifluoroethane (F113)7.7ND """"""Methylene chloride (Dichloromethane)3.5ND """"""Carbon disulfide 6.3ND """"""trans-1,2-Dichloroethene 8.0ND """"""1,1-Dichloroethane 4.1ND """"""2-Butanone (MEK)30ND """"""cis-1,2-Dichloroethene 4.0ND """"""Chloroform 4.9ND """"""1,1,1-Trichloroethane 5.5ND """"""1,2-Dichloroethane (EDC)4.1ND """"""Benzene 3.2ND """"""Carbon tetrachloride 6.4ND Page 5 of 13 Project: Project Number: Project Manager: Reported: SCS Engineers - San Diego 8799 Balboa Avenue, Suite 290 SCS111221-11 01221156.00/ 821 Main Street Luke MontagueSan Diego, CA 92123 16-Nov-21 15:37 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax H&P Mobile Geochemistry Inc. Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes Factor SV3-3 Rep (E111044-02) Vapor Sampled: 11-Nov-21 Received: 11-Nov-21 EPA TO-1515-Nov-21 15-Nov-21ug/m3 EK115081Trichloroethene5.5ND """"""1,2-Dichloropropane 9.4ND """"""Bromodichloromethane 6.8ND """"""cis-1,3-Dichloropropene 4.6ND """"""4-Methyl-2-pentanone (MIBK)8.3ND """"""trans-1,3-Dichloropropene 4.6ND """""Toluene "3.88.8 """"""1,1,2-Trichloroethane 5.5ND """"""2-Hexanone (MBK)8.3ND """"""Dibromochloromethane 8.6ND """"""Tetrachloroethene 6.9ND """"""1,2-Dibromoethane (EDB)7.8ND """"""1,1,1,2-Tetrachloroethane 7.0ND """"""Chlorobenzene 4.7ND """"""Ethylbenzene 4.4ND """"""m,p-Xylene 8.8ND """"""Styrene 4.3ND """"""o-Xylene 4.4ND """"""Bromoform 10ND """"""1,1,2,2-Tetrachloroethane 7.0ND """"""4-Ethyltoluene 5.0ND """"""1,3,5-Trimethylbenzene 5.0ND """"""1,2,4-Trimethylbenzene 5.0ND """"""1,3-Dichlorobenzene 12ND """"""1,4-Dichlorobenzene 12ND """"""1,2-Dichlorobenzene 12ND """"""1,2,4-Trichlorobenzene 38ND """"""Hexachlorobutadiene 54ND """"107 %76-134Surrogate: 1,2-Dichloroethane-d4 """"102 %78-125Surrogate: Toluene-d8 """"84.4 %77-127Surrogate: 4-Bromofluorobenzene Page 6 of 13 Project: Project Number: Project Manager: Reported: SCS Engineers - San Diego 8799 Balboa Avenue, Suite 290 SCS111221-11 01221156.00/ 821 Main Street Luke MontagueSan Diego, CA 92123 16-Nov-21 15:37 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax H&P Mobile Geochemistry Inc. Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes Factor SV2-2 (E111044-03) Vapor Sampled: 11-Nov-21 Received: 11-Nov-21 EPA TO-1515-Nov-21 15-Nov-21ug/m3 EK1150811,1-Difluoroethane (LCC)5.5ND """"""Dichlorodifluoromethane (F12)5.0ND """"""Chloromethane 2.1ND """"""Dichlorotetrafluoroethane (F114)7.1ND """"""Vinyl chloride 2.6ND """"""Bromomethane 16ND """"""Chloroethane 8.0ND """"""Trichlorofluoromethane (F11)5.6ND """"""1,1-Dichloroethene 4.0ND """"""1,1,2-Trichlorotrifluoroethane (F113)7.7ND """"""Methylene chloride (Dichloromethane)3.5ND """""Carbon disulfide "6.347 """"""trans-1,2-Dichloroethene 8.0ND """"""1,1-Dichloroethane 4.1ND """"""2-Butanone (MEK)30ND """"""cis-1,2-Dichloroethene 4.0ND """"""Chloroform 4.9ND """"""1,1,1-Trichloroethane 5.5ND """"""1,2-Dichloroethane (EDC)4.1ND """"""Benzene 3.2ND """"""Carbon tetrachloride 6.4ND """"""Trichloroethene 5.5ND """"""1,2-Dichloropropane 9.4ND """"""Bromodichloromethane 6.8ND """"""cis-1,3-Dichloropropene 4.6ND """"""4-Methyl-2-pentanone (MIBK)8.3ND """"""trans-1,3-Dichloropropene 4.6ND """""Toluene "3.819 """"""1,1,2-Trichloroethane 5.5ND """"""2-Hexanone (MBK)8.3ND """"""Dibromochloromethane 8.6ND """"""Tetrachloroethene 6.9ND """"""1,2-Dibromoethane (EDB)7.8ND """"""1,1,1,2-Tetrachloroethane 7.0ND """"""Chlorobenzene 4.7ND """"""Ethylbenzene 4.4ND """""m,p-Xylene "8.826 """"""Styrene 4.3ND Page 7 of 13 Project: Project Number: Project Manager: Reported: SCS Engineers - San Diego 8799 Balboa Avenue, Suite 290 SCS111221-11 01221156.00/ 821 Main Street Luke MontagueSan Diego, CA 92123 16-Nov-21 15:37 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax H&P Mobile Geochemistry Inc. Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes Factor SV2-2 (E111044-03) Vapor Sampled: 11-Nov-21 Received: 11-Nov-21 EK11508 15-Nov-21 15-Nov-21ug/m3 1o-Xylene EPA TO-154.47.2 """"""Bromoform 10ND """"""1,1,2,2-Tetrachloroethane 7.0ND """"""4-Ethyltoluene 5.0ND """"""1,3,5-Trimethylbenzene 5.0ND """""1,2,4-Trimethylbenzene "5.012 """"""1,3-Dichlorobenzene 12ND """"""1,4-Dichlorobenzene 12ND """"""1,2-Dichlorobenzene 12ND """"""1,2,4-Trichlorobenzene 38ND """"""Hexachlorobutadiene 54ND """"109 %76-134Surrogate: 1,2-Dichloroethane-d4 """"102 %78-125Surrogate: Toluene-d8 """"87.2 %77-127Surrogate: 4-Bromofluorobenzene SV1-4 (E111044-04) Vapor Sampled: 11-Nov-21 Received: 11-Nov-21 EPA TO-1515-Nov-21 15-Nov-21ug/m3 EK1150811,1-Difluoroethane (LCC)5.5ND """"""Dichlorodifluoromethane (F12)5.0ND """"""Chloromethane 2.1ND """"""Dichlorotetrafluoroethane (F114)7.1ND """"""Vinyl chloride 2.6ND """"""Bromomethane 16ND """"""Chloroethane 8.0ND """"""Trichlorofluoromethane (F11)5.6ND """"""1,1-Dichloroethene 4.0ND """"""1,1,2-Trichlorotrifluoroethane (F113)7.7ND """"""Methylene chloride (Dichloromethane)3.5ND """"""Carbon disulfide 6.3ND """"""trans-1,2-Dichloroethene 8.0ND """"""1,1-Dichloroethane 4.1ND """"""2-Butanone (MEK)30ND """"""cis-1,2-Dichloroethene 4.0ND """""Chloroform "4.99.0 """"""1,1,1-Trichloroethane 5.5ND """"""1,2-Dichloroethane (EDC)4.1ND """"""Benzene 3.2ND """"""Carbon tetrachloride 6.4ND Page 8 of 13 Project: Project Number: Project Manager: Reported: SCS Engineers - San Diego 8799 Balboa Avenue, Suite 290 SCS111221-11 01221156.00/ 821 Main Street Luke MontagueSan Diego, CA 92123 16-Nov-21 15:37 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax H&P Mobile Geochemistry Inc. Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes Factor SV1-4 (E111044-04) Vapor Sampled: 11-Nov-21 Received: 11-Nov-21 EPA TO-1515-Nov-21 15-Nov-21ug/m3 EK115081Trichloroethene5.5ND """"""1,2-Dichloropropane 9.4ND """"""Bromodichloromethane 6.8ND """"""cis-1,3-Dichloropropene 4.6ND """"""4-Methyl-2-pentanone (MIBK)8.3ND """"""trans-1,3-Dichloropropene 4.6ND """"""Toluene 3.8ND """"""1,1,2-Trichloroethane 5.5ND """"""2-Hexanone (MBK)8.3ND """"""Dibromochloromethane 8.6ND """"""Tetrachloroethene 6.9ND """"""1,2-Dibromoethane (EDB)7.8ND """"""1,1,1,2-Tetrachloroethane 7.0ND """"""Chlorobenzene 4.7ND """"""Ethylbenzene 4.4ND """"""m,p-Xylene 8.8ND """"""Styrene 4.3ND """"""o-Xylene 4.4ND """"""Bromoform 10ND """"""1,1,2,2-Tetrachloroethane 7.0ND """"""4-Ethyltoluene 5.0ND """"""1,3,5-Trimethylbenzene 5.0ND """"""1,2,4-Trimethylbenzene 5.0ND """"""1,3-Dichlorobenzene 12ND """"""1,4-Dichlorobenzene 12ND """"""1,2-Dichlorobenzene 12ND """"""1,2,4-Trichlorobenzene 38ND """"""Hexachlorobutadiene 54ND """"107 %76-134Surrogate: 1,2-Dichloroethane-d4 """"104 %78-125Surrogate: Toluene-d8 """"82.7 %77-127Surrogate: 4-Bromofluorobenzene Page 9 of 13 Project: Project Number: Project Manager: Reported: SCS Engineers - San Diego 8799 Balboa Avenue, Suite 290 SCS111221-11 01221156.00/ 821 Main Street Luke MontagueSan Diego, CA 92123 16-Nov-21 15:37 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax H&P Mobile Geochemistry Inc. Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by EPA TO-15 - Quality Control H&P Mobile Geochemistry, Inc. Batch EK11508 - TO-15 Blank (EK11508-BLK1)Prepared & Analyzed: 15-Nov-21 1,1-Difluoroethane (LCC)ug/m35.5ND Dichlorodifluoromethane (F12)"5.0ND Chloromethane "2.1ND Dichlorotetrafluoroethane (F114)"7.1ND Vinyl chloride "2.6ND Bromomethane "16ND Chloroethane "8.0ND Trichlorofluoromethane (F11)"5.6ND 1,1-Dichloroethene "4.0ND 1,1,2-Trichlorotrifluoroethane (F113)"7.7ND Methylene chloride (Dichloromethane)"3.5ND Carbon disulfide "6.3ND trans-1,2-Dichloroethene "8.0ND 1,1-Dichloroethane "4.1ND 2-Butanone (MEK)"30ND cis-1,2-Dichloroethene "4.0ND Chloroform "4.9ND 1,1,1-Trichloroethane "5.5ND 1,2-Dichloroethane (EDC)"4.1ND Benzene "3.2ND Carbon tetrachloride "6.4ND Trichloroethene "5.5ND 1,2-Dichloropropane "9.4ND Bromodichloromethane "6.8ND cis-1,3-Dichloropropene "4.6ND 4-Methyl-2-pentanone (MIBK)"8.3ND trans-1,3-Dichloropropene "4.6ND Toluene "3.8ND 1,1,2-Trichloroethane "5.5ND 2-Hexanone (MBK)"8.3ND Dibromochloromethane "8.6ND Tetrachloroethene "6.9ND 1,2-Dibromoethane (EDB)"7.8ND 1,1,1,2-Tetrachloroethane "7.0ND Page 10 of 13 Project: Project Number: Project Manager: Reported: SCS Engineers - San Diego 8799 Balboa Avenue, Suite 290 SCS111221-11 01221156.00/ 821 Main Street Luke MontagueSan Diego, CA 92123 16-Nov-21 15:37 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax H&P Mobile Geochemistry Inc. Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by EPA TO-15 - Quality Control H&P Mobile Geochemistry, Inc. Batch EK11508 - TO-15 Blank (EK11508-BLK1)Prepared & Analyzed: 15-Nov-21 Chlorobenzene ug/m34.7ND Ethylbenzene "4.4ND m,p-Xylene "8.8ND Styrene "4.3ND o-Xylene "4.4ND Bromoform "10ND 1,1,2,2-Tetrachloroethane "7.0ND 4-Ethyltoluene "5.0ND 1,3,5-Trimethylbenzene "5.0ND 1,2,4-Trimethylbenzene "5.0ND 1,3-Dichlorobenzene "12ND 1,4-Dichlorobenzene "12ND 1,2-Dichlorobenzene "12ND 1,2,4-Trichlorobenzene "38ND Hexachlorobutadiene "54ND "214 76-134Surrogate: 1,2-Dichloroethane-d4 107229 "208 78-125Surrogate: Toluene-d8 97.0202 "363 77-127Surrogate: 4-Bromofluorobenzene 82.0298 LCS (EK11508-BS1)Prepared & Analyzed: 15-Nov-21 Dichlorodifluoromethane (F12)ug/m3 101 QL-1H59-1281365.0140 Vinyl chloride "52.0 QL-1H64-1271412.673 Chloroethane "53.6 QL-1H63-1271348.072 Trichlorofluoromethane (F11)"113 62-1261085.6120 1,1-Dichloroethene "80.8 61-13385.04.069 1,1,2-Trichlorotrifluoroethane (F113)"155 66-1261037.7160 Methylene chloride (Dichloromethane)"70.8 62-11584.23.560 trans-1,2-Dichloroethene "80.8 67-12474.28.060 1,1-Dichloroethane "82.4 68-12681.34.167 cis-1,2-Dichloroethene "80.0 70-12176.24.061 Chloroform "99.2 68-12398.04.997 1,1,1-Trichloroethane "111 68-1251045.5120 1,2-Dichloroethane (EDC)"82.4 65-12897.34.180 Page 11 of 13 Project: Project Number: Project Manager: Reported: SCS Engineers - San Diego 8799 Balboa Avenue, Suite 290 SCS111221-11 01221156.00/ 821 Main Street Luke MontagueSan Diego, CA 92123 16-Nov-21 15:37 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax H&P Mobile Geochemistry Inc. Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by EPA TO-15 - Quality Control H&P Mobile Geochemistry, Inc. Batch EK11508 - TO-15 LCS (EK11508-BS1)Prepared & Analyzed: 15-Nov-21 Benzene ug/m3 64.8 69-11980.33.252 Carbon tetrachloride "128 68-1321106.4140 Trichloroethene "110 71-12395.65.5100 Toluene "76.8 66-11996.23.874 1,1,2-Trichloroethane "111 73-11986.85.596 Tetrachloroethene "138 66-12496.26.9130 1,1,1,2-Tetrachloroethane "140 67-1291017.0140 Ethylbenzene "88.4 70-12495.54.484 m,p-Xylene "88.4 61-1341018.889 o-Xylene "88.4 67-1251084.495 1,1,2,2-Tetrachloroethane "140 65-12777.37.0110 "214 76-134Surrogate: 1,2-Dichloroethane-d4 110234 "208 78-125Surrogate: Toluene-d8 98.0204 "363 77-127Surrogate: 4-Bromofluorobenzene 99.1360 Page 12 of 13 Project: Project Number: Project Manager: Reported: SCS Engineers - San Diego 8799 Balboa Avenue, Suite 290 SCS111221-11 01221156.00/ 821 Main Street Luke MontagueSan Diego, CA 92123 16-Nov-21 15:37 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax H&P Mobile Geochemistry Inc. Notes and Definitions QL-1H The LCS and/or LCSD recoveries fell above the established control specifications for this analyte. Any result for this compound is qualified and should be considered biased high. Percent Recovery Relative Percent DifferenceRPD %REC Method Detection LimitMDL Analyte NOT DETECTED at or above the reporting limitND Leak Check CompoundLCC Appendix H&P Mobile Geochemistry, Inc. is approved as an Environmental Testing Laboratory and Mobile Laboratory in accordance with the DoD -ELAP Program and ISO/IEC 17025:2005 programs through PJLA, accreditation number 69070 for EPA Method TO-15, EPA Method 8260B and H&P 8260SV. H&P is approved by the State of California as an Environmental Laboratory and Mobile Laboratory in conformance with the Environmental Laboratory Accreditation Program (ELAP) for the category of Volatile and Semi-Volatile Organic Chemistry of Hazardous Waste , certification numbers 2740, 2741, 2743 & 2745. H&P is approved by the State of Louisiana Department of Environmental Quality under the National Environmental Laboratory Accreditation Conference (NELAC) certification number 04138 The complete list of stationary and mobile laboratory certifications along with the fields of testing (FOTs) and analyte lists are available at www.handpmg.com/about/certifications. All soil results are reported in wet weight. Page 13 of 13 p Mobile Geochemistry, Inc. 2470 Impala Drive, Carlsbad, CA 92010 & Field Office - Signal Hill, CA W handpmg.com E info@handpmg.com P 760.804.9678 F 760.804.9159 VAPOR I AIR Chain of Custody DATE: 11111 7-1 Page i of Lab Client and Project Information Sample Receipt (Lab Use Only) Lab Client/Consultant:' nil 41.1te kr c Project Name / #: 617.7 _1Iscc,. 00 Date Rec'd: tit Li Control #. ;/.— VD-1(02.02- Lab Client Project Manager: LoLt, ,1 Project Location: _.2-1 i '-11,----ei2.71- H&P Project # sc s k. .D...k - 11 Lab Client Address: -7q47 B,A bccit 1Z240 1,2, ci 0 Report E-Mail(s): 6/, V71,1--n. i 64- I M4-),-/--6(..9 vevC) WS er-15 Av22,5- . c ail-, 0 cylect t ,P 3cs _ern; e-Lefb.-5-: c e--vi Lab Work Order # Ell' 011 44 Lab Client City, State, Zip: &.tb-, 11,er cin CA- clj_l 3---7 Sample Intact: Yes Notes Below See • No • Phone Number: -3 s 7 5. 7 I 55CD Receipt Gauge ID: (0. (s)..c)(o Temp: (2:A7-- Requirements Turnaround Time Reporting Sampler Information Outside Lab: Standard Report q Level III q Level IV q Excel EDD q Other EDD: Standard (7 day 05 `riei?irt,k'f6a0dr:g4 you . ary 1 )- re wk i 5 Sampler(s) Receipt Notes/Tracking #: Lab PM lni ials: ISWAre: kli e tie/.c47r) q CA Geotracker Global ID: X Rush (specify ate: 11 - 1 I— Z\ Additional Instructions to Laboratory: "Preferred VOC units (please choose one): q kug/L rsili µg/m3 q ppbv q ppmv LDVO C s St a n da r d Fu ll L i s t 82 60 S V { }TO - 15 VO C s S h o rt Li s t / Pr o j e c t Lis t El 82 6 0 S V 11 TO - 15 Ox y gen ate s q 82 6 0 S V E l TO - 15 Na p ht ha le n e q 826 0 S V q T O - 15 TP H v a s Ga s q 82 6 0 S V m q T O - 15 m Ar o m a t ic /A l ip ha tic F r a c t io n s q 82 6 0 S V m q T O - 15 m Le a k C h e c k C o mp ou nd DFA q I P A q H e Me tha ne by EP A 80 1 5 m Fi x e d G a s e s by AS T M D1 9 45 q CO2 L i 0 2 q N 2 SAMPLE NAME FIELD POINT NAME (if applicable) DATE mm/dd/yy TIME 24hr clock SAMPLE TYPE Indoor Air (IA), Ambient Air (AA), Subslab (SS), Soil Vapor (SV) CONTAINER SIZE & TYPE 400m1J1U6L Summa. Tedlar, Tube, etc. CO N T A I N E R ID ( ### ) La b u se o nly : Re c e ip t Va c 5143 - 5 II-H-21 65k '071 ;.(/,),,, 775 -Dlt Y X Srb- 30-ei o) 71( -k •tkl ->4 -)‹. VZ-7 r 11 21.3.0 -o .`to .> X '-)V - IA 4 ,....___ .„ 531 -o3' Y x. Approved/Relinquished by: 24/6.,, Company c 3-- Date: i 1)) 1/2 ITime: 1 le so Received b.y•___.....„...._________ Compan :4*p Date: 11 4 pi/ Time haj Approved/Relinquished . Company: Date: Time: Received by: Company: Date: Time: Approved/Relinquished by: Company: Date: Time: Received by: Company: Date: Time: *Approval constitutes as authorization to proceed with analysis and acceptance of conditions on back Appendix 6A1, Rev 1/9/2019, Effective 1/21/2019 SCS Engineers Project Name: 821 Main Street San Diego, CA 92123 8799 Balboa Avenue, Suite 290 Luke Montague Enclosed are the results of analyses for samples received by the laboratory on July 13, 2021. If you have any questions concerning this report, please feel free to contact us. 15 July 2021 Project ID: 1221156.00 Site Address: 821 Main Street Chula Vista, Ca American Scientific Laboratories, LLC (ASL) accepts sample materials from clients for analysis with the assumption that all of the information provided to ASL verbally or in writing by our clients (and/or their agents), regarding samples being submitted to ASL, is complete and accurate. ASL accepts all samples subject to the following conditions: 1) ASL is not responsible for verifying any client -provided information regarding any samples submitted to the laboratory. 2) ASL is not responsible for any consequences resulting from any inaccuracies , omissions, or misrepresentations contained in client-provided information regarding samples submitted to the laboratory. Work Order #: 2107069 Molky Brar Laboratory Director Page 1 of 22 Page 2 of 22 Page 3 of 22 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 1221156.00 Luke Montague 821 Main Street 07/15/2021 16:39San Diego CA, 92123 2107069Work Order No: ANALYTICAL SUMMARY REPORT Sample ID Laboratory ID Matrix Date Sampled Date Received SB1 2107069-01 Solid 07/13/2021 10:15 07/13/2021 13:45 SB2 2107069-02 Solid 07/13/2021 10:03 07/13/2021 13:45 SB3 2107069-03 Solid 07/13/2021 09:51 07/13/2021 13:45 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Amolk Brar, Lab Director Page 3 of 21Page 4 of 22 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 1221156.00 Luke Montague 821 Main Street 07/15/2021 16:39San Diego CA, 92123 2107069Work Order No: ResultAnalyte PQL Analyzed MethodNotes DilutionUnits Laboratory Sample ID: 2107069-01 (Solid) Prep Method Analyst Client Sample ID: SB1 Analytical Results Total Mercury (CVAA)Batch ID:BG10379 Prepared:07/14/2021 11:08 07/14/2021 16:45Mercury0.0500 mg/kg 1 7471A7471ALVEND Total ICP Metals Batch ID:BG10378 Prepared:07/14/2021 11:04 07/14/2021 16:15Antimony0.500 mg/kg 1 SW846 6010B3050BLVE0.699 07/14/2021 16:15Arsenic0.250 mg/kg 1 SW846 6010B3050BLVE5.10 07/14/2021 16:15Barium0.500 mg/kg 1 SW846 6010B3050BLVE111 07/14/2021 16:15Beryllium0.500 mg/kg 1 SW846 6010B3050BLVEND 07/14/2021 16:15Cadmium0.500 mg/kg 1 SW846 6010B3050BLVE1.43 07/14/2021 16:15Chromium0.500 mg/kg 1 SW846 6010B3050BLVE16.9 07/14/2021 16:15Cobalt0.500 mg/kg 1 SW846 6010B3050BLVE4.73 07/14/2021 16:15Copper0.500 mg/kg 1 SW846 6010B3050BLVE22.5 07/14/2021 16:15Lead0.250 mg/kg 1 SW846 6010B3050BLVE33.6 07/14/2021 16:15Molybdenum0.500 mg/kg 1 SW846 6010B3050BLVE1.00 07/14/2021 16:15Nickel0.500 mg/kg 1 SW846 6010B3050BLVE7.77 07/14/2021 16:15Selenium0.500 mg/kg 1 SW846 6010B3050BLVEND 07/14/2021 16:15Silver0.500 mg/kg 1 SW846 6010B3050BLVEND 07/14/2021 16:15Thallium0.500 mg/kg 1 SW846 6010B3050BLVEND 07/14/2021 16:15Vanadium0.500 mg/kg 1 SW846 6010B3050BLVE39.6 07/14/2021 16:15Zinc0.500 mg/kg 1 SW846 6010B3050BLVE170 Total Petroleum Hydrocarbons(TPH-g)Batch ID:BG10371 Prepared:07/14/2021 09:00 07/14/2021 13:34Gasoline Range Organics 500 ug/kg 1 8015B5030ASAND 07/14/2021 13:3470-120117 %Surrogate: Bromofluorobenzene 8015B5030ASA Total Petroleum Hydrocarbons(TPH DROORO)Batch ID:BG10373 Prepared:07/14/2021 09:00 07/14/2021 16:11Diesel range organics 10.0 mg/kg 1 8015B3550BSL74.0 07/14/2021 16:11Oil Range Organics 50.0 mg/kg 1 8015B3550BSL210 07/14/2021 16:1170-12092.1 %Surrogate: Chlorobenzene 8015B3550BSL The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Amolk Brar, Lab Director Page 4 of 21Page 5 of 22 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 1221156.00 Luke Montague 821 Main Street 07/15/2021 16:39San Diego CA, 92123 2107069Work Order No: ResultAnalyte PQL Analyzed MethodNotes DilutionUnits Laboratory Sample ID: 2107069-01 (Solid) Prep Method Analyst Client Sample ID: SB1 Analytical Results Volatile Organic Compounds Batch ID:BG10372 Prepared:07/14/2021 09:00 07/14/2021 15:41Acetone50.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41Benzene2.00 ug/kg 1 8260B5030ASAND 07/14/2021 15:41Bromobenzene10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41Bromochloromethane10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41Bromodichloromethane10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41Bromoform50.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41Bromomethane30.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:412-Butanone 50.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41n-Butylbenzene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41sec-Butylbenzene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41tert-Butylbenzene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41Carbon disulfide 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41Carbon tetrachloride 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41Chlorobenzene10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41Chloroethane30.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:412-Chloroethylvinyl Ether 50.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41Chloroform10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41Chloromethane30.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:414-Chlorotoluene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:412-Chlorotoluene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:411,2-Dibromo-3-chloropropane 50.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41Dibromochloromethane10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:411,2-Dibromoethane 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41Dibromomethane10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:411,2-Dichlorobenzene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:411,3-Dichlorobenzene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:411,4-Dichlorobenzene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41Dichlorodifluoromethane30.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:411,1-Dichloroethane 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:411,2-Dichloroethane 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:411,1-Dichloroethene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41cis-1,2-Dichloroethene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41trans-1,2-Dichloroethene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:411,1-Dichloropropene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:411,2-Dichloropropane 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:411,3-Dichloropropane 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:412,2-Dichloropropane 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41cis-1,3-Dichloropropene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41trans-1,3-Dichloropropene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41Ethylbenzene2.00 ug/kg 1 8260B5030ASAND The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Amolk Brar, Lab Director Page 5 of 21Page 6 of 22 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 1221156.00 Luke Montague 821 Main Street 07/15/2021 16:39San Diego CA, 92123 2107069Work Order No: ResultAnalyte PQL Analyzed MethodNotes DilutionUnits Laboratory Sample ID: 2107069-01 (Solid) Prep Method Analyst Client Sample ID: SB1 Analytical Results Volatile Organic Compounds Batch ID:BG10372 Prepared:07/14/2021 09:00 07/14/2021 15:41Hexachlorobutadiene30.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:412-Hexanone 50.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41Isopropylbenzene10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41p-Isopropyltoluene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41Methyl tert-Butyl Ether (MTBE)5.00 ug/kg 1 8260B5030ASAND 07/14/2021 15:414-Methyl-2-pentanone (MIBK)50.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41Methylene chloride 50.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41Naphthalene10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41n-Propylbenzene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41Styrene10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:411,1,1,2-Tetrachloroethane 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:411,1,2,2-Tetrachloroethane 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41Tetrachloroethene10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41Toluene2.00 ug/kg 1 8260B5030ASAND 07/14/2021 15:411,2,3-Trichlorobenzene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:411,2,4-Trichlorobenzene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:411,1,1-Trichloroethane 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:411,1,2-Trichloroethane 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41Trichloroethene10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41Trichlorofluoromethane10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:411,2,3-Trichloropropane 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:411,2,4-Trimethylbenzene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:411,3,5- Trimethylbenzene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41Vinyl acetate 50.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41Vinyl chloride 30.0 ug/kg 1 8260B5030ASAND 07/14/2021 15:41m,p-Xylenes 4.00 ug/kg 1 8260B5030ASAND 07/14/2021 15:41o-Xylene 2.00 ug/kg 1 8260B5030ASAND 07/14/2021 15:4170-120115 %Surrogate: 4-Bromofluorobenzene 8260B5030ASA 07/14/2021 15:4170-12074.6 %Surrogate: Dibromofluoromethane 8260B5030ASA 07/14/2021 15:4170-120105 %Surrogate: Toluene-d8 8260B5030ASA ResultAnalyte PQL Analyzed MethodNotes DilutionUnits Laboratory Sample ID: 2107069-02 (Solid) Prep Method Analyst Client Sample ID: SB2 Analytical Results Total Mercury (CVAA)Batch ID:BG10379 Prepared:07/14/2021 11:08 07/14/2021 16:45Mercury0.0500 mg/kg 1 7471A7471ALVEND The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Amolk Brar, Lab Director Page 6 of 21Page 7 of 22 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 1221156.00 Luke Montague 821 Main Street 07/15/2021 16:39San Diego CA, 92123 2107069Work Order No: ResultAnalyte PQL Analyzed MethodNotes DilutionUnits Laboratory Sample ID: 2107069-02 (Solid) Prep Method Analyst Client Sample ID: SB2 Analytical Results Total ICP Metals Batch ID:BG10378 Prepared:07/14/2021 11:04 07/14/2021 16:15Antimony0.500 mg/kg 1 SW846 6010B3050BLVEND 07/14/2021 16:15Arsenic0.250 mg/kg 1 SW846 6010B3050BLVE3.73 07/14/2021 16:15Barium0.500 mg/kg 1 SW846 6010B3050BLVE55.0 07/14/2021 16:15Beryllium0.500 mg/kg 1 SW846 6010B3050BLVEND 07/14/2021 16:15Cadmium0.500 mg/kg 1 SW846 6010B3050BLVE1.13 07/14/2021 16:15Chromium0.500 mg/kg 1 SW846 6010B3050BLVE12.7 07/14/2021 16:15Cobalt0.500 mg/kg 1 SW846 6010B3050BLVE4.61 07/14/2021 16:15Copper0.500 mg/kg 1 SW846 6010B3050BLVE25.3 07/14/2021 16:15Lead0.250 mg/kg 1 SW846 6010B3050BLVE7.99 07/14/2021 16:15Molybdenum0.500 mg/kg 1 SW846 6010B3050BLVE1.69 07/14/2021 16:15Nickel0.500 mg/kg 1 SW846 6010B3050BLVE5.20 07/14/2021 16:15Selenium0.500 mg/kg 1 SW846 6010B3050BLVEND 07/14/2021 16:15Silver0.500 mg/kg 1 SW846 6010B3050BLVEND 07/14/2021 16:15Thallium0.500 mg/kg 1 SW846 6010B3050BLVEND 07/14/2021 16:15Vanadium0.500 mg/kg 1 SW846 6010B3050BLVE35.3 07/14/2021 16:15Zinc0.500 mg/kg 1 SW846 6010B3050BLVE58.1 Total Petroleum Hydrocarbons(TPH-g)Batch ID:BG10371 Prepared:07/14/2021 09:00 07/14/2021 14:03Gasoline Range Organics 500 ug/kg 1 8015B5030ASAND 07/14/2021 14:0370-120117 %Surrogate: Bromofluorobenzene 8015B5030ASA Total Petroleum Hydrocarbons(TPH DROORO)Batch ID:BG10373 Prepared:07/14/2021 09:00 07/14/2021 15:28Diesel range organics 10.0 mg/kg 1 8015B3550BSL74.0 07/14/2021 15:28Oil Range Organics 50.0 mg/kg 1 8015B3550BSL290 07/14/2021 15:2870-12091.6 %Surrogate: Chlorobenzene 8015B3550BSL The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Amolk Brar, Lab Director Page 7 of 21Page 8 of 22 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 1221156.00 Luke Montague 821 Main Street 07/15/2021 16:39San Diego CA, 92123 2107069Work Order No: ResultAnalyte PQL Analyzed MethodNotes DilutionUnits Laboratory Sample ID: 2107069-02 (Solid) Prep Method Analyst Client Sample ID: SB2 Analytical Results Volatile Organic Compounds Batch ID:BG10372 Prepared:07/14/2021 09:00 07/14/2021 16:10Acetone50.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10Benzene2.00 ug/kg 1 8260B5030ASAND 07/14/2021 16:10Bromobenzene10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10Bromochloromethane10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10Bromodichloromethane10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10Bromoform50.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10Bromomethane30.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:102-Butanone 50.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10n-Butylbenzene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10sec-Butylbenzene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10tert-Butylbenzene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10Carbon disulfide 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10Carbon tetrachloride 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10Chlorobenzene10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10Chloroethane30.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:102-Chloroethylvinyl Ether 50.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10Chloroform10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10Chloromethane30.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:104-Chlorotoluene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:102-Chlorotoluene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:101,2-Dibromo-3-chloropropane 50.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10Dibromochloromethane10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:101,2-Dibromoethane 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10Dibromomethane10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:101,2-Dichlorobenzene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:101,3-Dichlorobenzene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:101,4-Dichlorobenzene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10Dichlorodifluoromethane30.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:101,1-Dichloroethane 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:101,2-Dichloroethane 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:101,1-Dichloroethene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10cis-1,2-Dichloroethene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10trans-1,2-Dichloroethene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:101,1-Dichloropropene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:101,2-Dichloropropane 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:101,3-Dichloropropane 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:102,2-Dichloropropane 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10cis-1,3-Dichloropropene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10trans-1,3-Dichloropropene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10Ethylbenzene2.00 ug/kg 1 8260B5030ASAND The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Amolk Brar, Lab Director Page 8 of 21Page 9 of 22 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 1221156.00 Luke Montague 821 Main Street 07/15/2021 16:39San Diego CA, 92123 2107069Work Order No: ResultAnalyte PQL Analyzed MethodNotes DilutionUnits Laboratory Sample ID: 2107069-02 (Solid) Prep Method Analyst Client Sample ID: SB2 Analytical Results Volatile Organic Compounds Batch ID:BG10372 Prepared:07/14/2021 09:00 07/14/2021 16:10Hexachlorobutadiene30.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:102-Hexanone 50.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10Isopropylbenzene10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10p-Isopropyltoluene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10Methyl tert-Butyl Ether (MTBE)5.00 ug/kg 1 8260B5030ASAND 07/14/2021 16:104-Methyl-2-pentanone (MIBK)50.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10Methylene chloride 50.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10Naphthalene10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10n-Propylbenzene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10Styrene10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:101,1,1,2-Tetrachloroethane 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:101,1,2,2-Tetrachloroethane 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10Tetrachloroethene10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10Toluene2.00 ug/kg 1 8260B5030ASAND 07/14/2021 16:101,2,3-Trichlorobenzene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:101,2,4-Trichlorobenzene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:101,1,1-Trichloroethane 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:101,1,2-Trichloroethane 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10Trichloroethene10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10Trichlorofluoromethane10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:101,2,3-Trichloropropane 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:101,2,4-Trimethylbenzene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:101,3,5- Trimethylbenzene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10Vinyl acetate 50.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10Vinyl chloride 30.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:10m,p-Xylenes 4.00 ug/kg 1 8260B5030ASAND 07/14/2021 16:10o-Xylene 2.00 ug/kg 1 8260B5030ASAND 07/14/2021 16:1070-12098.5 %Surrogate: 4-Bromofluorobenzene 8260B5030ASA 07/14/2021 16:1070-120100 %Surrogate: Dibromofluoromethane 8260B5030ASA 07/14/2021 16:1070-120108 %Surrogate: Toluene-d8 8260B5030ASA ResultAnalyte PQL Analyzed MethodNotes DilutionUnits Laboratory Sample ID: 2107069-03 (Solid) Prep Method Analyst Client Sample ID: SB3 Analytical Results Total Mercury (CVAA)Batch ID:BG10379 Prepared:07/14/2021 11:08 07/14/2021 16:45Mercury0.0500 mg/kg 1 7471A7471ALVEND The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Amolk Brar, Lab Director Page 9 of 21Page 10 of 22 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 1221156.00 Luke Montague 821 Main Street 07/15/2021 16:39San Diego CA, 92123 2107069Work Order No: ResultAnalyte PQL Analyzed MethodNotes DilutionUnits Laboratory Sample ID: 2107069-03 (Solid) Prep Method Analyst Client Sample ID: SB3 Analytical Results Total ICP Metals Batch ID:BG10378 Prepared:07/14/2021 11:04 07/14/2021 16:15Antimony0.500 mg/kg 1 SW846 6010B3050BLVEND 07/14/2021 16:15Arsenic0.250 mg/kg 1 SW846 6010B3050BLVE3.70 07/14/2021 16:15Barium0.500 mg/kg 1 SW846 6010B3050BLVE110 07/14/2021 16:15Beryllium0.500 mg/kg 1 SW846 6010B3050BLVEND 07/14/2021 16:15Cadmium0.500 mg/kg 1 SW846 6010B3050BLVE0.863 07/14/2021 16:15Chromium0.500 mg/kg 1 SW846 6010B3050BLVE5.79 07/14/2021 16:15Cobalt0.500 mg/kg 1 SW846 6010B3050BLVE3.82 07/14/2021 16:15Copper0.500 mg/kg 1 SW846 6010B3050BLVE5.87 07/14/2021 16:15Lead0.250 mg/kg 1 SW846 6010B3050BLVE7.33 07/14/2021 16:15Molybdenum0.500 mg/kg 1 SW846 6010B3050BLVEND 07/14/2021 16:15Nickel0.500 mg/kg 1 SW846 6010B3050BLVE3.13 07/14/2021 16:15Selenium0.500 mg/kg 1 SW846 6010B3050BLVEND 07/14/2021 16:15Silver0.500 mg/kg 1 SW846 6010B3050BLVEND 07/14/2021 16:15Thallium0.500 mg/kg 1 SW846 6010B3050BLVEND 07/14/2021 16:15Vanadium0.500 mg/kg 1 SW846 6010B3050BLVE26.7 07/14/2021 16:15Zinc0.500 mg/kg 1 SW846 6010B3050BLVE33.8 Total Petroleum Hydrocarbons(TPH-g)Batch ID:BG10371 Prepared:07/14/2021 09:00 07/14/2021 14:33Gasoline Range Organics 500 ug/kg 1 8015B5030ASAND 07/14/2021 14:3370-120108 %Surrogate: Bromofluorobenzene 8015B5030ASA Total Petroleum Hydrocarbons(TPH DROORO)Batch ID:BG10373 Prepared:07/14/2021 09:00 07/14/2021 14:45Diesel range organics 10.0 mg/kg 1 8015B3550BSLND 07/14/2021 14:45Oil Range Organics 50.0 mg/kg 1 8015B3550BSLND 07/14/2021 14:4570-12090.7 %Surrogate: Chlorobenzene 8015B3550BSL The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Amolk Brar, Lab Director Page 10 of 21Page 11 of 22 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 1221156.00 Luke Montague 821 Main Street 07/15/2021 16:39San Diego CA, 92123 2107069Work Order No: ResultAnalyte PQL Analyzed MethodNotes DilutionUnits Laboratory Sample ID: 2107069-03 (Solid) Prep Method Analyst Client Sample ID: SB3 Analytical Results Volatile Organic Compounds Batch ID:BG10372 Prepared:07/14/2021 09:00 07/14/2021 16:38Acetone50.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38Benzene2.00 ug/kg 1 8260B5030ASAND 07/14/2021 16:38Bromobenzene10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38Bromochloromethane10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38Bromodichloromethane10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38Bromoform50.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38Bromomethane30.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:382-Butanone 50.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38n-Butylbenzene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38sec-Butylbenzene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38tert-Butylbenzene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38Carbon disulfide 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38Carbon tetrachloride 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38Chlorobenzene10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38Chloroethane30.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:382-Chloroethylvinyl Ether 50.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38Chloroform10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38Chloromethane30.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:384-Chlorotoluene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:382-Chlorotoluene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:381,2-Dibromo-3-chloropropane 50.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38Dibromochloromethane10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:381,2-Dibromoethane 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38Dibromomethane10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:381,2-Dichlorobenzene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:381,3-Dichlorobenzene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:381,4-Dichlorobenzene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38Dichlorodifluoromethane30.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:381,1-Dichloroethane 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:381,2-Dichloroethane 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:381,1-Dichloroethene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38cis-1,2-Dichloroethene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38trans-1,2-Dichloroethene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:381,1-Dichloropropene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:381,2-Dichloropropane 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:381,3-Dichloropropane 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:382,2-Dichloropropane 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38cis-1,3-Dichloropropene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38trans-1,3-Dichloropropene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38Ethylbenzene2.00 ug/kg 1 8260B5030ASAND The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Amolk Brar, Lab Director Page 11 of 21Page 12 of 22 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 1221156.00 Luke Montague 821 Main Street 07/15/2021 16:39San Diego CA, 92123 2107069Work Order No: ResultAnalyte PQL Analyzed MethodNotes DilutionUnits Laboratory Sample ID: 2107069-03 (Solid) Prep Method Analyst Client Sample ID: SB3 Analytical Results Volatile Organic Compounds Batch ID:BG10372 Prepared:07/14/2021 09:00 07/14/2021 16:38Hexachlorobutadiene30.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:382-Hexanone 50.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38Isopropylbenzene10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38p-Isopropyltoluene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38Methyl tert-Butyl Ether (MTBE)5.00 ug/kg 1 8260B5030ASAND 07/14/2021 16:384-Methyl-2-pentanone (MIBK)50.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38Methylene chloride 50.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38Naphthalene10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38n-Propylbenzene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38Styrene10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:381,1,1,2-Tetrachloroethane 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:381,1,2,2-Tetrachloroethane 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38Tetrachloroethene10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38Toluene2.00 ug/kg 1 8260B5030ASAND 07/14/2021 16:381,2,3-Trichlorobenzene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:381,2,4-Trichlorobenzene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:381,1,1-Trichloroethane 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:381,1,2-Trichloroethane 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38Trichloroethene10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38Trichlorofluoromethane10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:381,2,3-Trichloropropane 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:381,2,4-Trimethylbenzene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:381,3,5- Trimethylbenzene 10.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38Vinyl acetate 50.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38Vinyl chloride 30.0 ug/kg 1 8260B5030ASAND 07/14/2021 16:38m,p-Xylenes 4.00 ug/kg 1 8260B5030ASAND 07/14/2021 16:38o-Xylene 2.00 ug/kg 1 8260B5030ASAND 07/14/2021 16:3870-120107 %Surrogate: 4-Bromofluorobenzene 8260B5030ASA 07/14/2021 16:3870-120103 %Surrogate: Dibromofluoromethane 8260B5030ASA 07/14/2021 16:3870-120108 %Surrogate: Toluene-d8 8260B5030ASA The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Amolk Brar, Lab Director Page 12 of 21Page 13 of 22 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 1221156.00 Luke Montague 821 Main Street 07/15/2021 16:39San Diego CA, 92123 2107069Work Order No: Result Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Total Mercury (CVAA) - Quality Control Report PQL Batch BG10379 - 7471A - 7471A Blank (BG10379-BLK1)Prepared & Analyzed: 07/14/202 Mercury mg/kg0.0500ND LCS (BG10379-BS1)Prepared & Analyzed: 07/14/202 Mercury mg/kg0.0500 0.100 80-1201080.108 LCS Dup (BG10379-BSD1)Prepared & Analyzed: 07/14/202 Mercury mg/kg0.0500 0.100 2080-120105 2.810.105 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Amolk Brar, Lab Director Page 13 of 21Page 14 of 22 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 1221156.00 Luke Montague 821 Main Street 07/15/2021 16:39San Diego CA, 92123 2107069Work Order No: Result Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Total ICP Metals - Quality Control Report PQL Batch BG10378 - 3050B - SW846 6010B Blank (BG10378-BLK1)Prepared & Analyzed: 07/14/202 Antimony mg/kg0.500ND Arsenic "0.250ND Barium "0.500ND Beryllium "0.500ND Cadmium "0.500ND Chromium "0.500ND Cobalt "0.500ND Copper "0.500ND Lead "0.250ND Molybdenum "0.500ND Nickel "0.500ND Selenium "0.500ND Silver "0.500ND Thallium "0.500ND Vanadium "0.500ND Zinc "0.500ND LCS (BG10378-BS1)Prepared & Analyzed: 07/14/202 Antimony mg/kg0.0100 1.00 80-12099.30.993 Arsenic "0.00500 1.00 80-12098.60.986 Barium "0.0100 1.00 80-1201041.04 Beryllium "0.0100 1.00 80-1201071.07 Cadmium "0.0100 1.00 80-12096.90.969 Chromium "0.0100 1.00 80-1201051.05 Cobalt "0.0100 1.00 80-1201001.00 Copper "0.0100 1.00 80-1201071.07 Lead "0.00500 1.00 80-1201001.00 Molybdenum "0.0100 1.00 80-1201021.02 Nickel "0.0100 1.00 80-1201011.01 Selenium "0.0100 1.00 80-12095.20.952 Silver "0.0100 1.00 80-1201001.00 Thallium "0.0100 1.00 80-12097.50.975 Vanadium "0.0100 1.00 80-1201021.02 Zinc "0.0100 1.00 80-1201051.05 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Amolk Brar, Lab Director Page 14 of 21Page 15 of 22 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 1221156.00 Luke Montague 821 Main Street 07/15/2021 16:39San Diego CA, 92123 2107069Work Order No: Result Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Total ICP Metals - Quality Control Report PQL Batch BG10378 - 3050B - SW846 6010B LCS Dup (BG10378-BSD1)Prepared & Analyzed: 07/14/202 Antimony mg/kg0.0100 1.00 2080-12085.3 15.10.853 Arsenic "0.00500 1.00 2080-12094.4 4.320.944 Barium "0.0100 1.00 2080-12098.3 5.390.983 Beryllium "0.0100 1.00 2080-120101 5.631.01 Cadmium "0.0100 1.00 2080-12094.0 3.060.940 Chromium "0.0100 1.00 2080-12099.6 5.690.996 Cobalt "0.0100 1.00 2080-12096.0 4.260.960 Copper "0.0100 1.00 2080-120101 6.011.01 Lead "0.00500 1.00 2080-12096.7 3.400.967 Molybdenum "0.0100 1.00 2080-12096.0 5.810.960 Nickel "0.0100 1.00 2080-12096.4 4.260.964 Selenium "0.0100 1.00 2080-12091.9 3.490.919 Silver "0.0100 1.00 2080-12096.6 3.730.966 Thallium "0.0100 1.00 2080-12095.4 2.090.954 Vanadium "0.0100 1.00 2080-12096.1 5.560.961 Zinc "0.0100 1.00 2080-120102 2.581.02 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Amolk Brar, Lab Director Page 15 of 21Page 16 of 22 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 1221156.00 Luke Montague 821 Main Street 07/15/2021 16:39San Diego CA, 92123 2107069Work Order No: Result Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Total Petroleum Hydrocarbons(TPH-g) - Quality Control Report PQL Batch BG10371 - 5030A - 8015B Blank (BG10371-BLK1)Prepared & Analyzed: 07/14/202 Gasoline Range Organics ug/kg500ND LCS (BG10371-BS1)Prepared & Analyzed: 07/14/202 Gasoline Range Organics ug/L 500 75-12098.1490 LCS Dup (BG10371-BSD1)Prepared & Analyzed: 07/14/202 Gasoline Range Organics ug/L 500 1575-12098.9 0.823494 Matrix Spike (BG10371-MS1)Prepared & Analyzed: 07/14/202Source: 2107069-01 Gasoline Range Organics ug/L 500 0.00 75-120100502 Matrix Spike Dup (BG10371-MSD1)Prepared & Analyzed: 07/14/202Source: 2107069-01 Gasoline Range Organics ug/L 500 0.00 1575-12091.7 9.06459 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Amolk Brar, Lab Director Page 16 of 21Page 17 of 22 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 1221156.00 Luke Montague 821 Main Street 07/15/2021 16:39San Diego CA, 92123 2107069Work Order No: Result Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Total Petroleum Hydrocarbons(TPH DROORO) - Quality Control Report PQL Batch BG10373 - 3550B - 8015B Blank (BG10373-BLK1)Prepared & Analyzed: 07/14/202 Diesel range organics mg/kg10.0ND Oil Range Organics "50.0ND mg/L 100 70-120Surrogate: Chlorobenzene 89.389.3 LCS (BG10373-BS1)Prepared & Analyzed: 07/14/202 Diesel range organics mg/L 500 75-120106528 "100 70-120Surrogate: Chlorobenzene 114114 LCS Dup (BG10373-BSD1)Prepared & Analyzed: 07/14/202 Diesel range organics mg/L 500 2075-12098.6 6.98493 "100 70-120Surrogate: Chlorobenzene 111111 Matrix Spike (BG10373-MS1)Prepared & Analyzed: 07/14/202Source: 2107069-01 Diesel range organics mg/L 500 74.0 75-12091.1529 "100 70-120Surrogate: Chlorobenzene 115115 Matrix Spike Dup (BG10373-MSD1)Prepared & Analyzed: 07/14/202Source: 2107069-01 Diesel range organics mg/L 500 74.0 2075-12085.7 5.23502 "100 70-120Surrogate: Chlorobenzene 112112 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Amolk Brar, Lab Director Page 17 of 21Page 18 of 22 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 1221156.00 Luke Montague 821 Main Street 07/15/2021 16:39San Diego CA, 92123 2107069Work Order No: Result Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds - Quality Control Report PQL Batch BG10372 - 5030A - 8260B Blank (BG10372-BLK1)Prepared & Analyzed: 07/14/202 Acetone ug/kg50.0ND Benzene "2.00ND Bromobenzene "10.0ND Bromochloromethane "10.0ND Bromodichloromethane "10.0ND Bromoform "50.0ND Bromomethane "30.0ND 2-Butanone "50.0ND n-Butylbenzene "10.0ND sec-Butylbenzene "10.0ND tert-Butylbenzene "10.0ND Carbon disulfide "10.0ND Carbon tetrachloride "10.0ND Chlorobenzene "10.0ND Chloroethane "30.0ND 2-Chloroethylvinyl Ether "50.0ND Chloroform "10.0ND Chloromethane "30.0ND 4-Chlorotoluene "10.0ND 2-Chlorotoluene "10.0ND 1,2-Dibromo-3-chloropropane "50.0ND Dibromochloromethane "10.0ND 1,2-Dibromoethane "10.0ND Dibromomethane "10.0ND 1,2-Dichlorobenzene "10.0ND 1,3-Dichlorobenzene "10.0ND 1,4-Dichlorobenzene "10.0ND Dichlorodifluoromethane "30.0ND 1,1-Dichloroethane "10.0ND 1,2-Dichloroethane "10.0ND 1,1-Dichloroethene "10.0ND cis-1,2-Dichloroethene "10.0ND trans-1,2-Dichloroethene "10.0ND 1,1-Dichloropropene "10.0ND 1,2-Dichloropropane "10.0ND 1,3-Dichloropropane "10.0ND 2,2-Dichloropropane "10.0ND cis-1,3-Dichloropropene "10.0ND trans-1,3-Dichloropropene "10.0ND Ethylbenzene "2.00ND Hexachlorobutadiene "30.0ND The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Amolk Brar, Lab Director Page 18 of 21Page 19 of 22 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 1221156.00 Luke Montague 821 Main Street 07/15/2021 16:39San Diego CA, 92123 2107069Work Order No: Result Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds - Quality Control Report PQL Batch BG10372 - 5030A - 8260B Blank (BG10372-BLK1)Prepared & Analyzed: 07/14/202 2-Hexanone ug/kg50.0ND Isopropylbenzene "10.0ND p-Isopropyltoluene "10.0ND Methyl tert-Butyl Ether (MTBE)"5.00ND 4-Methyl-2-pentanone (MIBK)"50.0ND Methylene chloride "50.0ND Naphthalene "10.0ND n-Propylbenzene "10.0ND Styrene "10.0ND 1,1,1,2-Tetrachloroethane "10.0ND 1,1,2,2-Tetrachloroethane "10.0ND Tetrachloroethene "10.0ND Toluene "2.00ND 1,2,3-Trichlorobenzene "10.0ND 1,2,4-Trichlorobenzene "10.0ND 1,1,1-Trichloroethane "10.0ND 1,1,2-Trichloroethane "10.0ND Trichloroethene "10.0ND Trichlorofluoromethane "10.0ND 1,2,3-Trichloropropane "10.0ND 1,2,4-Trimethylbenzene "10.0ND 1,3,5- Trimethylbenzene "10.0ND Vinyl acetate "50.0ND Vinyl chloride "30.0ND m,p-Xylenes "4.00ND o-Xylene "2.00ND LCS (BG10372-BS1)Prepared & Analyzed: 07/14/202 Benzene ug/L 50.0 75-12010251.2 Chlorobenzene "50.0 80-12010854.1 1,1-Dichloroethene "50.0 75-12010351.5 Methyl tert-Butyl Ether (MTBE)"50.0 75-12093.346.7 Toluene "50.0 75-12084.342.2 Trichloroethene "50.0 75-12094.747.4 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Amolk Brar, Lab Director Page 19 of 21Page 20 of 22 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 1221156.00 Luke Montague 821 Main Street 07/15/2021 16:39San Diego CA, 92123 2107069Work Order No: Result Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds - Quality Control Report PQL Batch BG10372 - 5030A - 8260B LCS Dup (BG10372-BSD1)Prepared & Analyzed: 07/14/202 Benzene ug/L 50.0 2075-120102 0.25451.1 Chlorobenzene "50.0 2080-120107 1.0253.6 1,1-Dichloroethene "50.0 1575-120106 2.6252.9 Methyl tert-Butyl Ether (MTBE)"50.0 1575-12093.0 0.36546.5 Toluene "50.0 1575-12084.8 0.61542.4 Trichloroethene "50.0 2075-12094.3 0.46647.2 Matrix Spike (BG10372-MS1)Prepared & Analyzed: 07/14/202Source: 2107056-01 Benzene ug/L 50.0 0.140 75-12010452.4 Chlorobenzene "50.0 0.00 75-12010954.7 1,1-Dichloroethene "50.0 0.00 75-12011055.0 Methyl tert-Butyl Ether (MTBE)"50.0 0.00 75-12010954.7 Toluene "50.0 0.00 75-12085.742.8 Trichloroethene "50.0 0.00 75-12097.348.6 Matrix Spike Dup (BG10372-MSD1)Prepared & Analyzed: 07/14/202Source: 2107056-01 Benzene ug/L 50.0 0.140 1575-120106 1.2053.0 Chlorobenzene "50.0 0.00 1575-120112 1.9755.8 1,1-Dichloroethene "50.0 0.00 1575-120119 7.6659.4 Methyl tert-Butyl Ether (MTBE)"50.0 0.00 1575-120120 9.5460.2 Toluene "50.0 0.00 1575-12086.8 1.2543.4 Trichloroethene "50.0 0.00 1575-12098.1 0.86049.1 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety . Amolk Brar, Lab Director Page 20 of 21Page 21 of 22 Project: Project Number: Project Manager: Reported: SCS Engineers 8799 Balboa Avenue, Suite 290 1221156.00 Luke Montague 821 Main Street 07/15/2021 16:39San Diego CA, 92123 2107069Work Order No: Notes and Definitions Sample results reported on a dry weight basis Relative Percent DifferenceRPD dry Not ReportedNR Analyte NOT DETECTED at or above the practical quantitation limit (PQL)ND Analyte DETECTEDDET Page 22 of 22